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  1. Article ; Online: Micro solid phase extraction of lead and cadmium using functionalized nanodiamonds@CuAl

    Soylak, Mustafa / Çoban, Ayşe Nur / Ahmed, Hassan Elzain Hassan

    Food chemistry

    2024  Volume 442, Page(s) 138426

    Abstract: This study focuses on the development and application of a novel nanocomposite (functionalized nanodiamonds@ ... ...

    Abstract This study focuses on the development and application of a novel nanocomposite (functionalized nanodiamonds@CuAl
    MeSH term(s) Cadmium/analysis ; Nanodiamonds ; Lead ; Nanocomposites ; Solid Phase Extraction/methods ; Water ; Spectrophotometry, Atomic/methods ; Metal-Organic Frameworks
    Chemical Substances Cadmium (00BH33GNGH) ; Nanodiamonds ; bis(1,3,5-benzenetricarboxylate)tricopper(II) ; Lead (2P299V784P) ; Water (059QF0KO0R) ; Metal-Organic Frameworks
    Language English
    Publishing date 2024-01-14
    Publishing country England
    Document type Journal Article
    ZDB-ID 243123-3
    ISSN 1873-7072 ; 0308-8146
    ISSN (online) 1873-7072
    ISSN 0308-8146
    DOI 10.1016/j.foodchem.2024.138426
    Database MEDical Literature Analysis and Retrieval System OnLINE

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  2. Article: Arsenic speciation by using emerging sample preparation techniques: a review.

    Jagirani, Muhammad Saqaf / Soylak, Mustafa

    Turkish journal of chemistry

    2023  Volume 47, Issue 5, Page(s) 991–1006

    Abstract: Arsenic is a hazardous element that causes environmental pollution. Due to its toxicological effects, it is crucial to quantify and minimize the hazardous impact on the ecology. Despite the significant advances in analytical techniques, sample ... ...

    Abstract Arsenic is a hazardous element that causes environmental pollution. Due to its toxicological effects, it is crucial to quantify and minimize the hazardous impact on the ecology. Despite the significant advances in analytical techniques, sample preparation is still crucial for determining target analytes in complex matrices. Several factors affect the direct analysis, such as trace-level analysis, advanced regulatory requirements, complexity of sample matrices, and incompatible with analytical instrumentation. Along with the development in the sample preparation process, microextraction methods play an essential role in the sample preparation process. Microextraction techniques (METs) are the newest green approach that replaces traditional sample preparation and preconcentration methods. METs have minimized the limitation of conventional sample preparation methods while keeping all their benefits. METs improve extraction efficacy, are fast, automated, use less amount of solvents, and are suitable for the environment. Microextraction techniques with less solvent consumption, such as solid phase microextraction (SPME) solvent-free methods, and liquid phase microextraction (LPME), are widely used in modern analytical procedures. SPME development focuses on synthesizing new sorbents and applying online sample preparation, whereas LPME research investigates the utilization of new solvents.
    Language English
    Publishing date 2023-06-23
    Publishing country Turkey
    Document type Journal Article
    ZDB-ID 2046471-X
    ISSN 1303-6130 ; 1300-0527
    ISSN (online) 1303-6130
    ISSN 1300-0527
    DOI 10.55730/1300-0527.3590
    Database MEDical Literature Analysis and Retrieval System OnLINE

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  3. Article ; Online: Novel reusable and switchable deep eutectic solvent for extraction and determination of curcumin in water and food samples.

    Salamat, Qamar / Soylak, Mustafa

    Talanta

    2023  Volume 269, Page(s) 125401

    Abstract: For the first time, a fast and easy extraction method based on a unique reusable and switchable deep eutectic solvent (made of octylamine, succinic acid, and water as precursors) was presented and utilized for the microextraction and determination of ... ...

    Abstract For the first time, a fast and easy extraction method based on a unique reusable and switchable deep eutectic solvent (made of octylamine, succinic acid, and water as precursors) was presented and utilized for the microextraction and determination of curcumin as a model analyte. The main factors used to induce a phase transition in the as-prepared deep eutectic solvent were solutions of NaOH and HCl. Among the standout characteristics of the suggested deep eutectic solvent are the removal of toxic organic solvents like THF, the lack of a need for centrifugation, and the ability to be reused in subsequent extractions. The influence of effective parameters (i.e., proportions of deep eutectic solvent structure components, volume of prepared deep eutectic solvent, volume and concertation of NaOH, volume of HCl, and salt effect) on the extraction procedure were investigated. The calibration curve also was linear in the range of 35-500 μg L
    MeSH term(s) Solvents/chemistry ; Water/chemistry ; Curcumin/analysis ; Deep Eutectic Solvents ; Sodium Hydroxide ; Limit of Detection ; Liquid Phase Microextraction/methods
    Chemical Substances Solvents ; Water (059QF0KO0R) ; Curcumin (IT942ZTH98) ; Deep Eutectic Solvents ; Sodium Hydroxide (55X04QC32I)
    Language English
    Publishing date 2023-11-10
    Publishing country Netherlands
    Document type Journal Article
    ZDB-ID 1500969-5
    ISSN 1873-3573 ; 0039-9140
    ISSN (online) 1873-3573
    ISSN 0039-9140
    DOI 10.1016/j.talanta.2023.125401
    Database MEDical Literature Analysis and Retrieval System OnLINE

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  4. Article ; Online: Carboxylated nanodiamonds@CuAl

    Soylak, Mustafa / Aksu, Birgul / Elzain Hassan Ahmed, Hassan

    Food chemistry

    2024  Volume 445, Page(s) 138733

    Abstract: Heavy metal pollution poses a significant health risk, necessitating regular environmental monitoring for public safety. Elevated nickel concentrations can disrupt ecosystems and impact human health. This study presents a nano-sorbent can be used for ... ...

    Abstract Heavy metal pollution poses a significant health risk, necessitating regular environmental monitoring for public safety. Elevated nickel concentrations can disrupt ecosystems and impact human health. This study presents a nano-sorbent can be used for dispersive micro-solid phase extraction of nickel. The nano-sorbent was characterized using FT-IR, XRD, FESEM, BET, and BJH. It demonstrated remarkable efficiency due to its nanoscale properties, optimizing results in exceptional extraction performance with minimal interference from common ions. A flame atomic absorption spectrometer was utilized for all measurements. It has a low LOD (0.29 μg L
    MeSH term(s) Animals ; Humans ; Nickel ; Nanodiamonds ; Spectroscopy, Fourier Transform Infrared ; Ecosystem ; Nanocomposites ; Water ; Solid Phase Extraction/methods
    Chemical Substances Nickel (7OV03QG267) ; Nanodiamonds ; Water (059QF0KO0R)
    Language English
    Publishing date 2024-02-14
    Publishing country England
    Document type Journal Article
    ZDB-ID 243123-3
    ISSN 1873-7072 ; 0308-8146
    ISSN (online) 1873-7072
    ISSN 0308-8146
    DOI 10.1016/j.foodchem.2024.138733
    Database MEDical Literature Analysis and Retrieval System OnLINE

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  5. Article ; Online: Ultrasound assisted magnetic solid phase extraction of copper(II) and lead(II) in environmental samples on Magnetic Activated Carbon Cloth

    Soylak, Mustafa / Maulana, Rizqan

    International Journal of Environmental Analytical Chemistry. 2023 Sept. 02, v. 103, no. 11 p.2542-2554

    2023  

    Abstract: Copper (II) and lead (II) ions are complexed with 1-nitroso-2-naphthol and preconcentrated on the magnetic activated carbon cloth prior to its flame atomic absorption spectrometric detection. Analytical parameters such as model solution pH, adsorbent ... ...

    Abstract Copper (II) and lead (II) ions are complexed with 1-nitroso-2-naphthol and preconcentrated on the magnetic activated carbon cloth prior to its flame atomic absorption spectrometric detection. Analytical parameters such as model solution pH, adsorbent amount, eluent type and volume, ligand amount, sample volume and matrix effect were determined. As a result of these studies, quantitative recovery of analyte ions was obtained at pH 4.0. Quantitative recovery was observed with 2 mL 3 M HNO₃ solution as eluent. The developed method has been applied to various water and food samples and the accuracy of the developed method has been confirmed by certified reference material analysis and addition recovery studies. The method has been applied to the separation and preconcentration of copper (II) and lead (II) ions in water and food samples.
    Keywords activated carbon ; adsorbents ; analytical chemistry ; atomic absorption spectrometry ; copper ; lead ; ligands ; magnetism ; pH ; reference standards ; solid phase extraction ; ultrasonics ; Magnetic activated carbon cloth ; 1-nitroso-2-naphthol ; micro sampling flame atomic absorption spectrometry
    Language English
    Dates of publication 2023-0902
    Size p. 2542-2554.
    Publishing place Taylor & Francis
    Document type Article ; Online
    ZDB-ID 120480-4
    ISSN 1029-0397 ; 0306-7319 ; 0092-9085
    ISSN (online) 1029-0397
    ISSN 0306-7319 ; 0092-9085
    DOI 10.1080/03067319.2021.1895136
    Database NAL-Catalogue (AGRICOLA)

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  6. Article ; Online: Metal-organic framework functionalized with deep eutectic solvent for solid-phase extraction of Rhodamine 6G in water and cosmetic products.

    Ozalp, Ozgur / Gumus, Zinar Pinar / Soylak, Mustafa

    Journal of separation science

    2023  Volume 46, Issue 19, Page(s) e2300190

    Abstract: ... An ... ...

    Abstract An NH
    Language English
    Publishing date 2023-07-26
    Publishing country Germany
    Document type Journal Article
    ZDB-ID 2047990-6
    ISSN 1615-9314 ; 1615-9306
    ISSN (online) 1615-9314
    ISSN 1615-9306
    DOI 10.1002/jssc.202300190
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  7. Article ; Online: A magnetic solid phase extraction procedure for Pb(II) at trace levels on magnetic Luffa@TiO

    Ahmed, Hassan Elzain Hassan / Mohammed, Ali Mohammednour Ali / Soylak, Mustafa

    Food chemistry

    2023  Volume 428, Page(s) 136794

    Abstract: A novel magnetic Luffa@ ... ...

    Abstract A novel magnetic Luffa@TiO
    MeSH term(s) Animals ; Cattle ; Luffa ; Lead ; Solid Phase Extraction/methods ; Water ; Adsorption ; Magnetic Phenomena ; Spectrophotometry, Atomic/methods ; Water Pollutants, Chemical/analysis
    Chemical Substances Lead (2P299V784P) ; 1,4-thiomorpholine-3,5-dicarboxylic acid (91828-95-4) ; titanium dioxide (15FIX9V2JP) ; Water (059QF0KO0R) ; Water Pollutants, Chemical
    Language English
    Publishing date 2023-07-04
    Publishing country England
    Document type Journal Article
    ZDB-ID 243123-3
    ISSN 1873-7072 ; 0308-8146
    ISSN (online) 1873-7072
    ISSN 0308-8146
    DOI 10.1016/j.foodchem.2023.136794
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  8. Article ; Online: Fe

    Soylak, Mustafa / Uzcan, Furkan / Goktas, Oguzhan / Gumus, Zinar Pinar

    Food chemistry

    2023  Volume 429, Page(s) 136855

    Abstract: A magnetic metal-organic framework ... ...

    Abstract A magnetic metal-organic framework Fe
    MeSH term(s) Cadmium/analysis ; Silicon Dioxide ; Solid Phase Extraction/methods ; Nanocomposites/chemistry ; Magnetic Phenomena
    Chemical Substances Cadmium (00BH33GNGH) ; Silicon Dioxide (7631-86-9)
    Language English
    Publishing date 2023-07-13
    Publishing country England
    Document type Journal Article
    ZDB-ID 243123-3
    ISSN 1873-7072 ; 0308-8146
    ISSN (online) 1873-7072
    ISSN 0308-8146
    DOI 10.1016/j.foodchem.2023.136855
    Database MEDical Literature Analysis and Retrieval System OnLINE

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  9. Article: Supramolecular solvents: a review of a modern innovation in liquid-phase microextraction technique.

    Jagirani, Muhammad Saqaf / Soylak, Mustafa

    Turkish journal of chemistry

    2021  Volume 45, Issue 6, Page(s) 1651–1677

    Abstract: Supramolecular solvents (SUPRASs) have rapidly gained more attention as a potential substitute to organic solvents in the sample preparation and preconcentration process. The essential properties of SUPRAS solvents (e.g., multiple binding sites, ... ...

    Abstract Supramolecular solvents (SUPRASs) have rapidly gained more attention as a potential substitute to organic solvents in the sample preparation and preconcentration process. The essential properties of SUPRAS solvents (e.g., multiple binding sites, different polarity microenvironments, the opportunity to tailor their properties, etc.) these qualities offer numerous opportunities to advance innovative sample preparation and pretreatment platforms compared to the traditional solvents. Among these qualities, certain importance is placed on theoretical and practical knowledge. That has assisted in making significant developments in SUPRAS that advance our understanding of the processes behind SUPRA'S formation. The SUPRA-solute interactions that drive extractions are explored in this context to develop knowledge-based extraction techniques. This review mainly focused on the significant application of supramolecular-based solvents (SUPRASs) in microextraction techniques. SUPRASs-based liquid-phase microextraction (LPME) is an excellent tool for extracting, simple preparation, and preconcentration from complex environmental samples. SUPRASs-LPME has a wide range of applications for analyzing food, environmental samples, pharmaceuticals, and biological samples.
    Language English
    Publishing date 2021-11-29
    Publishing country Turkey
    Document type Journal Article ; Review
    ZDB-ID 2046471-X
    ISSN 1303-6130 ; 1300-0527
    ISSN (online) 1303-6130
    ISSN 1300-0527
    DOI 10.3906/kim-2110-15
    Database MEDical Literature Analysis and Retrieval System OnLINE

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  10. Article ; Online: Advanced Methodologies for Trace Elements in Edible Oil Samples: A Review.

    Shah, Nasrullah Syed / Soylak, Mustafa

    Critical reviews in analytical chemistry

    2021  Volume 52, Issue 7, Page(s) 1572–1582

    Abstract: Advanced methodologies were applied for the detection of some elements at trace levels in edible oils. Trace elements play a role in oil stability, quality of edible oils and fats. In the present study, problems were addressed related to simple, cheap, ... ...

    Abstract Advanced methodologies were applied for the detection of some elements at trace levels in edible oils. Trace elements play a role in oil stability, quality of edible oils and fats. In the present study, problems were addressed related to simple, cheap, less time consuming and suitable pretreatment advanced methods for suitable sample introduction and calibrations as well as the strategies and techniques are discussed. The present review is aimed to discuss the significance of simplifying sample treatments are offered for trace elements in oils. The period covered by this review is last twenty years. However, the various applications of advanced methodologies including extraction and microextraction. The scope of spectrometric techniques used for the analysis of trace elements in edible oils was discussed by new instrumental development trends.
    MeSH term(s) Plant Oils/analysis ; Plant Oils/chemistry ; Trace Elements/analysis
    Chemical Substances Plant Oils ; Trace Elements
    Language English
    Publishing date 2021-03-15
    Publishing country United States
    Document type Journal Article ; Review
    ZDB-ID 2030019-0
    ISSN 1547-6510 ; 1040-8347
    ISSN (online) 1547-6510
    ISSN 1040-8347
    DOI 10.1080/10408347.2021.1895710
    Database MEDical Literature Analysis and Retrieval System OnLINE

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