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Article: Dr. L. O. Howard.

WADE, J S

2004 Volume 166, Issue 4220, Page(s) 460–461

MeSH term(s)	History, 19th Century ; History, 20th Century ; Humans
Language	English
Publishing date	2004-01-12
Publishing country	England
Document type	Biography ; Historical Article ; Journal Article
ZDB-ID	120714-3
ISSN	1476-4687 ; 0028-0836
ISSN (online)	1476-4687
ISSN	0028-0836
DOI	10.1038/166460a0
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Article ; Online: A late-transition metal oxo complex: K7Na9[O=PtIV(H2O)L2], L = [PW9O34]9-.

Anderson, Travis M / Neiwert, Wade A / Kirk, Martin L / Piccoli, Paula M B / Schultz, Arthur J / Koetzle, Thomas F / Musaev, Djamaladdin G / Morokuma, Keiji / Cao, Rui / Hill, Craig L

publication RETRACTED

Science (New York, N.Y.)

2004 Volume 306, Issue 5704, Page(s) 2074–2077

Abstract: ... orbitals. A platinum(IV)-oxo compound flanked by two polytungstate ligands, K7Na9[O=Pt(H2O)L2], L = [PW9O34 ... neutron diffraction at 30 kelvin revealed a very short [1.720(18) angstrom] Pt-O bond and no evidence of a hydrogen ...

Abstract	Terminal mono-oxo complexes of the late transition metal elements have long been considered too unstable to synthesize because of repulsion between the oxygen electrons and the mostly filled metal d orbitals. A platinum(IV)-oxo compound flanked by two polytungstate ligands, K7Na9[O=Pt(H2O)L2], L = [PW9O34(9-)], has now been prepared and isolated at room temperature as air-stable brown crystals. X-ray and neutron diffraction at 30 kelvin revealed a very short [1.720(18) angstrom] Pt-O bond and no evidence of a hydrogen atom at the terminal oxygen, ruling out a better precedented Pt-OH complex. Density functional theory and spectroscopic data account for the stability of the Pt(IV)-oxo unit by electron withdrawal into delocalized orbitals of the polytungstates.
MeSH term(s)	Chemical Phenomena ; Chemistry, Physical ; Crystallization ; Crystallography, X-Ray ; Electrons ; Fourier Analysis ; Hydrogen-Ion Concentration ; Ligands ; Molecular Structure ; Neutron Diffraction ; Oxidation-Reduction ; Oxygen/chemistry ; Platinum/chemistry ; Platinum Compounds/chemical synthesis ; Platinum Compounds/chemistry ; Platinum Compounds/isolation & purification ; Spectrum Analysis ; Temperature ; Tungsten/chemistry ; Tungsten Compounds/chemical synthesis ; Tungsten Compounds/chemistry ; Tungsten Compounds/isolation & purification
Chemical Substances	Ligands ; Platinum Compounds ; Tungsten Compounds ; potassium sodium diaquaoxobis(PW9O34)platinum(IV) ; Platinum (49DFR088MY) ; Oxygen (S88TT14065) ; Tungsten (V9306CXO6G)
Language	English
Publishing date	2004-12-17
Publishing country	United States
Document type	Journal Article ; Research Support, U.S. Gov't, Non-P.H.S. ; Research Support, U.S. Gov't, P.H.S. ; Retracted Publication
ZDB-ID	128410-1
ISSN	1095-9203 ; 0036-8075
ISSN (online)	1095-9203
ISSN	0036-8075
DOI	10.1126/science.1104696
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Article: A Late-Transition Metal Oxo Complex: KâNaâ[O=Pt[superscript IV](HâO)Lâ], L = [PWâOââ]â¹â»

Anderson, Travis M / Cao, Rui / Hill, Craig L / Kirk, Martin L / Koetzle, Thomas F / Morokuma, Keiji / Musaev, Djamaladdin G / Neiwert, Wade A / Piccoli, Paula M. B / Schultz, Arthur J

Science. 2004 Dec. 17, v. 306, no. 5704

2004

Abstract: ... orbitals. A platinum(IV)-oxo compound flanked by two polytungstate ligands, KâNaâ[O=Pt(HâO)Lâ], L ... crystals. X-ray and neutron diffraction at 30 kelvin revealed a very short [1.720(18) angstrom] Pt-O bond ...

Abstract	Terminal mono-oxo complexes of the late transition metal elements have long been considered too unstable to synthesize because of repulsion between the oxygen electrons and the mostly filled metal d orbitals. A platinum(IV)-oxo compound flanked by two polytungstate ligands, KâNaâ[O=Pt(HâO)Lâ], L = [PWâOâââ¹â»], has now been prepared and isolated at room temperature as air-stable brown crystals. X-ray and neutron diffraction at 30 kelvin revealed a very short [1.720(18) angstrom] Pt-O bond and no evidence of a hydrogen atom at the terminal oxygen, ruling out a better precedented Pt-OH complex. Density functional theory and spectroscopic data account for the stability of the Pt(IV)-oxo unit by electron withdrawal into delocalized orbitals of the polytungstates.
Keywords	ambient temperature ; crystals ; electrons ; hydrogen ; ligands ; oxygen ; platinum ; spectral analysis ; X-ray diffraction
Language	English
Dates of publication	2004-1217
Size	p. 2074-2077.
Document type	Article
ZDB-ID	128410-1
ISSN	1095-9203 ; 0036-8075
ISSN (online)	1095-9203
ISSN	0036-8075
DOI	10.1126/science.1104696
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Article ; Online: Management of Neuroendocrine Ductal Carcinoma In Situ of the Breast.

Ma, Brenda L / Rooks, Clayton O / Christopher, Wade O / Berry, Scott M

The American surgeon

2023 Volume 89, Issue 8, Page(s) 3526–3527

Abstract: Neuroendocrine tumors are defined as tumors that express neuroendocrine markers, specifically synaptophysin and/or chromogranin in at least 50% of tumor cells. To date, neuroendocrine cancers of the breast are extremely rare with reports that they ... ...

Abstract	Neuroendocrine tumors are defined as tumors that express neuroendocrine markers, specifically synaptophysin and/or chromogranin in at least 50% of tumor cells. To date, neuroendocrine cancers of the breast are extremely rare with reports that they account for less than 1% of all neuroendocrine tumors and less than .1% of all breast cancers. Limited literature exists to guide treatment decisions tailored to neuroendocrine tumors of the breast, despite the possibility that they may be associated with an overall worse prognosis. We present a rare case of neuroendocrine ductal carcinoma in situ (NE-DCIS) which was discovered upon workup for bloody nipple discharge. In this case, NE-DCIS was managed with the standard recommended treatment regimen for ductal carcinoma in situ.
MeSH term(s)	Humans ; Female ; Carcinoma, Intraductal, Noninfiltrating/surgery ; Carcinoma, Intraductal, Noninfiltrating/pathology ; Breast/pathology ; Breast Neoplasms/surgery ; Breast Neoplasms/pathology ; Carcinoma, Neuroendocrine/surgery ; Carcinoma, Neuroendocrine/pathology ; Neuroendocrine Tumors/diagnosis ; Neuroendocrine Tumors/surgery
Language	English
Publishing date	2023-03-03
Publishing country	United States
Document type	Case Reports ; Journal Article
ZDB-ID	202465-2
ISSN	1555-9823 ; 0003-1348
ISSN (online)	1555-9823
ISSN	0003-1348
DOI	10.1177/00031348231161080
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Article ; Online: Patient-reported outcome measures for primary hyperparathyroidism: a systematic review of measurement properties.

Liang, George / Kaur, Manraj N / Wade, Carrie G / Edelen, Maria O / Bates, David W / Pusic, Andrea L / Liu, Jason B

Health and quality of life outcomes

2024 Volume 22, Issue 1, Page(s) 31

Abstract: Background: The quality of patient-reported outcome measures (PROMs) used to assess the outcomes of primary hyperparathyroidism (PHPT), a common endocrine disorder that can negatively affect patients' health-related quality of life due to chronic ... ...

Abstract	Background: The quality of patient-reported outcome measures (PROMs) used to assess the outcomes of primary hyperparathyroidism (PHPT), a common endocrine disorder that can negatively affect patients' health-related quality of life due to chronic symptoms, has not been rigorously examined. This systematic review aimed to summarize and evaluate evidence on the measurement properties of PROMs used in adult patients with PHPT, and to provide recommendations for appropriate measure selection. Methods: After PROSPERO registration (CRD42023438287), Medline, EMBASE, CINAHL Complete, Web of Science, PsycINFO, and Cochrane Trials were searched for full-text articles in English investigating PROM development, pilot studies, or evaluation of at least one PROM measurement property in adult patients with any clinical form of PHPT. Two reviewers independently identified studies for inclusion and conducted the review following the Consensus-Based Standards for the Selection of Health Measurement Instruments (COSMIN) Methodology to assess risk of bias, evaluate the quality of measurement properties, and grade the certainty of evidence. Results: From 4989 records, nine PROM development or validation studies were identified for three PROMs: the SF-36, PAS, and PHPQoL. Though the PAS demonstrated sufficient test-retest reliability and convergent validity, and the PHPQoL sufficient test-retest reliability, convergent validity, and responsiveness, the certainty of evidence was low-to-very low due to risk of bias. All three PROMs lacked sufficient evidence for content validity in patients with PHPT. Conclusions: Based upon the available evidence, the SF-36, PAS, and PHPQoL cannot currently be recommended for use in research or clinical care, raising important questions about the conclusions of studies using these PROMs. Further validation studies or the development of more relevant PROMs with strong measurement properties for this patient population are needed.
MeSH term(s)	Adult ; Humans ; Quality of Life ; Reproducibility of Results ; Hyperparathyroidism, Primary ; Patient Reported Outcome Measures ; Consensus
Language	English
Publishing date	2024-04-02
Publishing country	England
Document type	Systematic Review ; Journal Article ; Review
ZDB-ID	2098765-1
ISSN	1477-7525 ; 1477-7525
ISSN (online)	1477-7525
ISSN	1477-7525
DOI	10.1186/s12955-024-02248-9
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Article: 3-O-methyldopa uptake and inhibition of L-dopa at the blood-brain barrier.

Wade, L A / Katzman, R

Life sciences

1975 Volume 17, Issue 1, Page(s) 131–136

MeSH term(s)	Animals ; Biological Availability ; Biological Transport, Active ; Blood-Brain Barrier ; Brain/metabolism ; Cerebral Cortex/metabolism ; Corpus Striatum/metabolism ; Diffusion ; Hypothalamus/metabolism ; Kinetics ; Levodopa/antagonists & inhibitors ; Levodopa/therapeutic use ; Male ; Mesencephalon/metabolism ; Methyldopa/blood ; Methyldopa/metabolism ; Parkinson Disease/drug therapy ; Rats
Chemical Substances	Levodopa (46627O600J) ; Methyldopa (56LH93261Y)
Language	English
Publishing date	1975-07-01
Publishing country	Netherlands
Document type	Journal Article
ZDB-ID	3378-9
ISSN	1879-0631 ; 0024-3205
ISSN (online)	1879-0631
ISSN	0024-3205
DOI	10.1016/0024-3205(75)90248-9
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Article ; Online: Zinc detection in oil-polluted marine environment by stripping voltammetry with mercury-free nanoporous gold electrode.

Clochard, M-C / Oral, O / Wade, T L / Cavani, O / Castellino, M / Ligiero, L Medina / Elan, T

Scientific reports

2022 Volume 12, Issue 1, Page(s) 15771

Abstract: ... constant of 1.41 L [Formula: see text]mol[Formula: see text] and a maximum Zn(II) adsorbed mass q[Formula ... concentrations ranging from 10 to 500 [Formula: see text]g L[Formula: see text] and 100 to 1000 [Formula: see ... text]g L[Formula: see text] respectively. The LOD was 4.2 [Formula: see text]g L[Formula: see text] (3S ...

Abstract	Detection of Zn(II) in oil-polluted seawater via square-wave anodic stripping voltammetry (SW-ASV) utilizing thin gold electrodes sputtered onto nanoporous poly(acrylic acid)-grafted-poly(vinylidene difluoride) (PAA-g-PVDF) membrane is herein reported. Prior to SW-ASV, PAA grafted nanopores demonstrated to efficiently trap Zn(II) ions at open circuit. This passive adsorption followed a Langmuir law. An affinity constant of 1.41 L [Formula: see text]mol[Formula: see text] and a maximum Zn(II) adsorbed mass q[Formula: see text] of 1.21 [Formula: see text]mol g[Formula: see text] were found. Applied SW-ASV protocol implied an accumulation step (- 1.2 V for 120 s) followed by a stripping step (- 1.2 to 1 V; 25 Hz; step: 4 mV; amplitude: 25 mV; acetate buffer (pH 5.5)). It revealed a Zn redox potential at - 0.8 V (Ag/AgCl pseudo-reference). Multiple measurements in synthetic waters close to the composition of production waters exhibited a decreasing precision with the number of readings R (1.65[Formula: see text] (R = 2) and 6.56[Formula: see text] (R = 3)). These membrane-electrodes should be used as disposable. The intra-batch mean precision was 14[Formula: see text] (n = 3) while inter-batches precision was 20[Formula: see text] (n = 15). Linear and linear-log calibrations allow exploitation of Zn(II) concentrations ranging from 10 to 500 [Formula: see text]g L[Formula: see text] and 100 to 1000 [Formula: see text]g L[Formula: see text] respectively. The LOD was 4.2 [Formula: see text]g L[Formula: see text] (3S/N). Thanks to obtained calibration, a detected Zn(II) content of 1 ppm in a raw production water from North Sea oil platform was determined.
MeSH term(s)	Electrochemistry/methods ; Electrodes ; Gold ; Ions ; Mercury/chemistry ; Nanopores ; Water/chemistry ; Zinc/chemistry
Chemical Substances	Ions ; Water (059QF0KO0R) ; Gold (7440-57-5) ; Mercury (FXS1BY2PGL) ; Zinc (J41CSQ7QDS)
Language	English
Publishing date	2022-09-21
Publishing country	England
Document type	Journal Article ; Research Support, Non-U.S. Gov't
ZDB-ID	2615211-3
ISSN	2045-2322 ; 2045-2322
ISSN (online)	2045-2322
ISSN	2045-2322
DOI	10.1038/s41598-022-20067-0
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Article ; Online: Network meta-analysis of CAR T-Cell therapy for the treatment of 3L+ R/R LBCL after using published comparative studies.

Oluwole, Olalekan O / Neelapu, Sattva S / Ray, Markqayne D / Limbrick-Oldfield, Eve H / Wade, Sally W / Kanters, Steve / Patel, Anik R / Locke, Frederick L

Expert review of anticancer therapy

2024 , Page(s) 1–9

Abstract: Introduction: Studies have compared chimeric antigen receptor (CAR) T-cell therapies and salvage chemotherapy in relapsed/refractory large B-cell lymphoma (LBCL) patients, but further evidence of their relative effectiveness is warranted.: Methods: ... ...

Abstract	Introduction: Studies have compared chimeric antigen receptor (CAR) T-cell therapies and salvage chemotherapy in relapsed/refractory large B-cell lymphoma (LBCL) patients, but further evidence of their relative effectiveness is warranted. Methods: Our systematic review identified studies comparing efficacy and safety outcomes of axicabtagene ciloleucel (axi-cel), lisocabtagene maraleucel (liso-cel) and tisagenlecleucel (tisa-cel) trials to salvage chemotherapy cohorts in LBCL patients with ≥2 prior lines of treatment; and an extended evidence network included indirect comparisons comparing CAR T-cell therapies. We conducted network meta-analyzes using Bayesian hierarchical modeling. Results: Three studies comparing ZUMA-1 (axi-cel), TRANSCEND (liso-cel) and JULIET (tisa-cel) trials to salvage chemotherapy within the SCHOLAR-1 cohort were identified. Axi-cel (odds ratio [OR]:5.63; 95% credible interval [CrI]:2.66-12.42) and liso-cel (OR:4.26; 95%CrI:2.33-7.93) showed a significant increased overall response rate compared to tisa-cel, but not to one-another. Axi-cel demonstrated significant improvements in overall survival relative to liso-cel (hazard ratio [HR]:0.54; 95%CrI:0.37-0.79) and tisa-cel (HR:0.47; 95%CrI:0.26-0.88). Higher rates of grade ≥3 neurological events were observed with axi-cel than with tisa-cel and liso-cel. Conclusions: We highlight important differences in clinical outcomes between CAR T-cell therapies. Axi-cel demonstrated improved overall survival compared to tisa-cel and liso-cel, and both axi-cel and liso-cel showed higher response rates compared to tisa-cel.
Language	English
Publishing date	2024-04-24
Publishing country	England
Document type	Journal Article ; Review
ZDB-ID	2112544-2
ISSN	1744-8328 ; 1473-7140
ISSN (online)	1744-8328
ISSN	1473-7140
DOI	10.1080/14737140.2024.2343801
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Article: The Use and Impact of Antibiotics in Plant Agriculture: A Review.

Batuman, Ozgur / Britt-Ugartemendia, Kellee / Kunwar, Sanju / Yilmaz, Salih / Fessler, Lauren / Redondo, Ana / Chumachenko, Kseniya / Chakravarty, Shourish / Wade, Tara

Phytopathology

2024

Abstract: Growers have depended on the specificity and efficacy of streptomycin and oxytetracycline as a part of their plant disease arsenal since the middle of the twentieth century. With climate change intensifying plant bacterial epidemics, the established ... ...

Abstract	Growers have depended on the specificity and efficacy of streptomycin and oxytetracycline as a part of their plant disease arsenal since the middle of the twentieth century. With climate change intensifying plant bacterial epidemics, the established success of these antibiotics remains threatened. Our strong reliance on certain antibiotics for devastating diseases eventually gave way to resistance development. Though antibiotics in plant agriculture equal to less than 0.5% of overall antibiotic use in the US, it is still imperative for humans to continue to monitor usage, environmental residues, and resistance in bacterial populations. This review provides an overview of the history and use, resistance and mitigation, regulation, environmental impact, and economics of antibiotics in plant agriculture. Bacterial issues, such as the ongoing Huanglongbing (citrus greening) epidemic in Florida citrus production, may need antibiotics for adequate control. Therefore, preserving the efficacy of our current antibiotics by utilizing more targeted application methods, such as trunk injection, should be a major focus.
Language	English
Publishing date	2024-03-13
Publishing country	United States
Document type	Journal Article
ZDB-ID	208889-7
ISSN	1943-7684 ; 0031-949X
ISSN (online)	1943-7684
ISSN	0031-949X
DOI	10.1094/PHYTO-10-23-0357-IA
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Article: Assessment of aeration control strategies for biofilm-based partial nitritation/anammox systems.

Schraa, O / Rosenthal, A / Wade, M J / Rieger, L / Miletić, I / Alex, J

Water science and technology : a journal of the International Association on Water Pollution Research

2020 Volume 81, Issue 8, Page(s) 1757–1765

Abstract: The objective of this work was to compare the nitrogen removal in mainstream, biofilm-based partial nitritation anammox (PN/A) systems employing (1) constant setpoint dissolved oxygen (DO) control, (2) intermittent aeration, and (3) ammonia-based ... ...

Abstract	The objective of this work was to compare the nitrogen removal in mainstream, biofilm-based partial nitritation anammox (PN/A) systems employing (1) constant setpoint dissolved oxygen (DO) control, (2) intermittent aeration, and (3) ammonia-based aeration control (ABAC). A detailed water resource recovery facility (WRRF) model was used to study the dynamic performance of these aeration control strategies with respect to treatment performance and energy consumption. The results show that constant setpoint DO control cannot meet typical regulatory limits for total ammonia nitrogen (NH
MeSH term(s)	Ammonia ; Biofilms ; Bioreactors ; Nitrogen ; Oxidation-Reduction
Chemical Substances	Ammonia (7664-41-7) ; Nitrogen (N762921K75)
Language	English
Publishing date	2020-07-21
Publishing country	England
Document type	Journal Article
ZDB-ID	764273-8
ISSN	1996-9732 ; 0273-1223
ISSN (online)	1996-9732
ISSN	0273-1223
DOI	10.2166/wst.2020.174
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