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Article: Effects of Geographical Origin and Tree Age on the Stable Isotopes and Multi-Elements of Pu-erh Tea.

Chen, Ming-Ming / Liao, Qiu-Hong / Qian, Li-Li / Zou, Hai-Dan / Li, Yan-Long / Song, Yan / Xia, Yu / Liu, Yi / Liu, Hong-Yan / Liu, Ze-Long

Foods (Basel, Switzerland)

2024 Volume 13, Issue 3

Abstract: Pu-erh tea is a famous tea worldwide, and identification of the geographical origin of Pu-erh tea ... may also influence the fingerprints of Pu-erh tea. In order to study the effects of the geographical origin ... and tree age on the interactions of stable isotopes and multi-elements of Pu-erh tea, 53 Pu-erh tea ...

Abstract	Pu-erh tea is a famous tea worldwide, and identification of the geographical origin of Pu-erh tea can not only protect manufacture's interests, but also boost consumers' confidence. However, tree age may also influence the fingerprints of Pu-erh tea. In order to study the effects of the geographical origin and tree age on the interactions of stable isotopes and multi-elements of Pu-erh tea, 53 Pu-erh tea leaves with three different age stages from three different areas in Yunnan were collected in 2023. The δ
Language	English
Publishing date	2024-02-02
Publishing country	Switzerland
Document type	Journal Article
ZDB-ID	2704223-6
ISSN	2304-8158
ISSN	2304-8158
DOI	10.3390/foods13030473
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Article ; Online: Rheological and Aging Properties of Vegetable Oil-Based Polyurethane (V-PU) Modified Asphalt.

Xia, Lei / Cao, Dongwei / Zhang, Hongliang

Polymers

2023 Volume 15, Issue 9

Abstract: To study the rheological and aging properties of vegetable oil-based polyurethane (V-PU) modified ... asphalt, V-PU terminated with an -NCO group was synthesized from renewable castor oil, and liquefied MDI ... 100LL and 10-40 wt% V-PU modified asphalts were prepared. Temperature classification, multiple stress ...

Abstract	To study the rheological and aging properties of vegetable oil-based polyurethane (V-PU) modified asphalt, V-PU terminated with an -NCO group was synthesized from renewable castor oil, and liquefied MDI-100LL and 10-40 wt% V-PU modified asphalts were prepared. Temperature classification, multiple stress creep recovery (MSCR), and linear amplitude scanning (LAS) tests were carried out. The results showed that the modulus, the creep recovery rate (R), and the yield stress and yield strain of the V-PU modified asphalts significantly increased in the order: 0 wt% < 10 wt% < 20 wt% < 40 wt% < 30 wt%, while the phase angle and the unrecoverable creep compliance (Jnr) changed in the opposite order, and the high temperature grade of 30 wt% V-PU modified asphalt was 4 grades higher than that of the base asphalt, which indicated that the addition of V-PU enhanced the fatigue, permanent deformation, and recovery deformation resistance. The 30 wt% sample exhibited phase inversion had the best performance. Comprehensive FTIR, GPC, and fluorescence microscopy analyses showed that the molecular weight significantly increased and the V-PU molecules agglomerated after aging. The excess -NCO groups of V-PU prepolymer react with water in the air and the active hydrogen in the asphalt system and finally form a cross-linked three-dimensional network structure with the asphalt to improve performance. The mechanism of intramolecular cementation reaction and the aging process of V-PU modified asphalt was creatively derived.
Language	English
Publishing date	2023-04-30
Publishing country	Switzerland
Document type	Journal Article
ZDB-ID	2527146-5
ISSN	2073-4360 ; 2073-4360
ISSN (online)	2073-4360
ISSN	2073-4360
DOI	10.3390/polym15092158
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Article ; Online: A wearable sweat electrochemical aptasensor based on the Ni-Co MOF nanosheet-decorated CNTs/PU film for monitoring of stress biomarker.

Su, Tong / Mi, Ziyi / Xia, Youyuan / Jin, Dangqin / Xu, Qin / Hu, Xiaoya / Shu, Yun

Talanta

2023 Volume 260, Page(s) 124620

Abstract: ... CNTs)/polyurethane (PU) film is developed for rapid and reliable detection of cortisol in sweat. First ... the CNTs/PU (CP) film was prepared by a modified wet spinning technology, and the CNTs/polyvinyl alcohol ...

Abstract	Monitoring cortisol, a hormone released by the adrenal cortex in response to stress, is essential to evaluate the endocrine response to stress stimuli. While the current cortisol sensing methods require large laboratory settings, complex assay, and professional personnel. Herein, a novel flexible and wearable electrochemical aptasensor based on a Ni-Co metal-organic frameworks (MOF) nanosheet-decorated carbon nanotubes (CNTs)/polyurethane (PU) film is developed for rapid and reliable detection of cortisol in sweat. First, the CNTs/PU (CP) film was prepared by a modified wet spinning technology, and the CNTs/polyvinyl alcohol (PVA) solution was thermally deposited on the surface of CP film to form the highly flexible CNTs/PVA/CP (CCP) film with excellent conductivity. Then aminated Ni-Co MOF nanosheet prepared by a facile solvothermal method was conjugated with streptavidin and modified on the CCP film. Biofunctional MOF can effectively capture cortisol aptamer due to its excellent specific surface area. In addition, the MOF with peroxidase activity can catalytic oxidization of hydroquinone (HQ) by hydrogen peroxide (H
MeSH term(s)	Humans ; Metal-Organic Frameworks ; Nanotubes, Carbon ; Sweat ; Polyurethanes ; Hydrocortisone ; Hydrogen Peroxide ; Wearable Electronic Devices ; Biosensing Techniques/methods ; Electrochemical Techniques/methods
Chemical Substances	Metal-Organic Frameworks ; Nanotubes, Carbon ; Polyurethanes ; Hydrocortisone (WI4X0X7BPJ) ; Hydrogen Peroxide (BBX060AN9V)
Language	English
Publishing date	2023-05-02
Publishing country	Netherlands
Document type	Journal Article
ZDB-ID	1500969-5
ISSN	1873-3573 ; 0039-9140
ISSN (online)	1873-3573
ISSN	0039-9140
DOI	10.1016/j.talanta.2023.124620
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Article ; Online: Intermediate occupation numbers for 5f electrons in a Pu and U mixed oxide.

Li, Ru-Song / Xie, Zheng / Kong, Ling-Yun / Hou, Su-Xia / Luo, Ji-Jun / Xin, Du-Qiang

Physical chemistry chemical physics : PCCP

2021 Volume 23, Issue 27, Page(s) 14725–14736

Abstract: ... occupation numbers of Pu/U ions in a (Pu,U) mixed oxide-PuUO4, a first principles calculation is performed ... orbit coupling (SOC) and on-site Coulomb repulsion for correlation effect due to localized Pu/U 5f ... orbitals. Results demonstrate that Pu/U 5f electron occupation numbers in the ground state of PuUO4 are ...

Abstract	In order to reveal the correlation effect on the electronic properties in particular 5f electron occupation numbers of Pu/U ions in a (Pu,U) mixed oxide-PuUO4, a first principles calculation is performed by using density functional theory (DFT) plus a dynamical mean field theory (DMFT) scheme with the spin-orbit coupling (SOC) and on-site Coulomb repulsion for correlation effect due to localized Pu/U 5f orbitals. Results demonstrate that Pu/U 5f electron occupation numbers in the ground state of PuUO4 are mainly composed of 5f4/5f5 and 5f2/5f3 configurations, and exhibiting the intermediate occupation (IO) numbers with average 5f occupation numbers of about nf = 4.879 and 2.423 for Pu and U ions, respectively, irrespective of different Pu and U lattice sites in PuUO4. Pu 5f j = 5/2 and j = 7/2 components are in moderately and weakly correlated states, respectively, while U 5f j = 5/2 and j = 7/2 manifolds are both in weakly correlated states. jj and LS coupling schemes are feasible for Pu and U 5f electrons, respectively. In order to directly compare with the experimental angle-resolved photoemission spectrum (ARPES), we also estimate the momentum-resolved electronic spectrum function for this system.
Language	English
Publishing date	2021-06-30
Publishing country	England
Document type	Journal Article
ZDB-ID	1476244-4
ISSN	1463-9084 ; 1463-9076
ISSN (online)	1463-9084
ISSN	1463-9076
DOI	10.1039/d1cp01149a
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Article ; Online: Differentiating Pu-erh raw tea from different geographical origins by

Wu, Xia / Liu, Ying / Guo, Jieqing / Wang, Juanxia / Li, Meizhen / Tan, Youzhen / Zheng, Qifan / Feng, Yifan

Journal of food science

2021 Volume 86, Issue 3, Page(s) 779–791

Abstract: Pu-erh tea is believed to be a beneficial beverage for health due to its many kinds ... of pharmacological effects. Nevertheless, detailed information related to differences in metabolites of Pu-erh raw ... in water-soluble components of Pu-erh raw tea by highly sensitive ultra-performance liquid chromatography ...

Abstract	Pu-erh tea is believed to be a beneficial beverage for health due to its many kinds of pharmacological effects. Nevertheless, detailed information related to differences in metabolites of Pu-erh raw tea from different geographical origins remains scarce. In this study, 43 elements were found in water-soluble components of Pu-erh raw tea by highly sensitive ultra-performance liquid chromatography quadrupole time-of-flight mass spectrometry (U-HPLC/Q-TOF-MS). The characteristic groups of 29 metabolites from nondestructive proton nuclear magnetic resonance (
MeSH term(s)	Camellia sinensis/chemistry ; Camellia sinensis/classification ; Catechin ; Chromatography, High Pressure Liquid ; Discriminant Analysis ; Flavonoids/analysis ; Least-Squares Analysis ; Magnetic Resonance Spectroscopy ; Mass Spectrometry ; Plant Extracts/chemistry ; Tea/chemistry ; Tea/classification
Chemical Substances	Flavonoids ; Plant Extracts ; Tea ; epiafzelechin ; Catechin (8R1V1STN48)
Language	English
Publishing date	2021-02-18
Publishing country	United States
Document type	Journal Article
ZDB-ID	241615-3
ISSN	1750-3841 ; 0022-1147
ISSN (online)	1750-3841
ISSN	0022-1147
DOI	10.1111/1750-3841.15624
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Article ; Online: Highly sensitive piezoresistive and thermally responsive fibrous networks from the in situ growth of PEDOT on MWCNT-decorated electrospun PU fibers for pressure and temperature sensing.

Luo, Yunyun / Zhao, Libo / Luo, Guoxi / Dong, Linxi / Xia, Yong / Li, Min / Li, Ziping / Wang, Kaifei / Maeda, Ryutaro / Jiang, Zhuangde

Microsystems & nanoengineering

2023 Volume 9, Page(s) 113

Abstract: ... ultrasonication treatment and in situ polymerization growth. Electrospun polyurethane (PU) microfibers were anchored ... PEDOT) was grown on the surface of PU fibers decorated with MWCNTs to enhance the conductive ... the PEDOT/MWCNT@PU mat-based device exhibits a wide working range (0-70 kPa), high sensitivity (1.6 kPa ...

Abstract	Flexible electronics have demonstrated various strategies to enhance the sensory ability for tactile perception and wearable physiological monitoring. Fibrous microstructures have attracted much interest because of their excellent mechanical properties and fabricability. Herein, a structurally robust fibrous mat was first fabricated by electrospinning, followed by a sequential process of functionalization utilizing ultrasonication treatment and in situ polymerization growth. Electrospun polyurethane (PU) microfibers were anchored with multi-walled carbon nanotubes (MWCNTs) to form conductive paths along each fiber by a scalable ultrasonic cavitation treatment in an MWCNT suspension. After, a layer of poly(3,4-ethylene dioxythiophene) (PEDOT) was grown on the surface of PU fibers decorated with MWCNTs to enhance the conductive conjunctions of MWCNTs. Due to the superior electromechanical behaviors and mechanical reinforcement of PEDOT, the PEDOT/MWCNT@PU mat-based device exhibits a wide working range (0-70 kPa), high sensitivity (1.6 kPa
Language	English
Publishing date	2023-09-15
Publishing country	England
Document type	Journal Article
ISSN	2055-7434
ISSN (online)	2055-7434
DOI	10.1038/s41378-023-00593-1
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Article ; Online: Joint Determination of Reactor Antineutrino Spectra from ^{235}U and ^{239}Pu Fission by Daya Bay and PROSPECT.

An, F P / Andriamirado, M / Balantekin, A B / Band, H R / Bass, C D / Bergeron, D E / Berish, D / Bishai, M / Blyth, S / Bowden, N S / Bryan, C D / Cao, G F / Cao, J / Chang, J F / Chang, Y / Chen, H S / Chen, S M / Chen, Y / Chen, Y X /

Cheng, J / Cheng, Z K / Cherwinka, J J / Chu, M C / Classen, T / Conant, A J / Cummings, J P / Dalager, O / Deichert, G / Delgado, A / Deng, F S / Ding, Y Y / Diwan, M V / Dohnal, T / Dolinski, M J / Dolzhikov, D / Dove, J / Dvořák, M / Dwyer, D A / Erickson, A / Foust, B T / Gaison, J K / Galindo-Uribarri, A / Gallo, J P / Gilbert, C E / Gonchar, M / Gong, G H / Gong, H / Grassi, M / Gu, W Q / Guo, J Y / Guo, L / Guo, X H / Guo, Y H / Guo, Z / Hackenburg, R W / Hans, S / Hansell, A B / He, M / Heeger, K M / Heffron, B / Heng, Y K / Hor, Y K / Hsiung, Y B / Hu, B Z / Hu, J R / Hu, T / Hu, Z J / Huang, H X / Huang, J H / Huang, X T / Huang, Y B / Huber, P / Koblanski, J / Jaffe, D E / Jayakumar, S / Jen, K L / Ji, X L / Ji, X P / Johnson, R A / Jones, D C / Kang, L / Kettell, S H / Kohn, S / Kramer, M / Kyzylova, O / Lane, C E / Langford, T J / LaRosa, J / Lee, J / Lee, J H C / Lei, R T / Leitner, R / Leung, J K C / Li, F / Li, H L / Li, J J / Li, Q J / Li, R H / Li, S / Li, S C / Li, W D / Li, X N / Li, X Q / Li, Y F / Li, Z B / Liang, H / Lin, C J / Lin, G L / Lin, S / Ling, J J / Link, J M / Littenberg, L / Littlejohn, B R / Liu, J C / Liu, J L / Liu, J X / Lu, C / Lu, H Q / Lu, X / Luk, K B / Ma, B Z / Ma, X B / Ma, X Y / Ma, Y Q / Mandujano, R C / Maricic, J / Marshall, C / McDonald, K T / McKeown, R D / Mendenhall, M P / Meng, Y / Meyer, A M / Milincic, R / Mueller, P E / Mumm, H P / Napolitano, J / Naumov, D / Naumova, E / Neilson, R / Nguyen, T M T / Nikkel, J A / Nour, S / Ochoa-Ricoux, J P / Olshevskiy, A / Palomino, J L / Pan, H-R / Park, J / Patton, S / Peng, J C / Pun, C S J / Pushin, D A / Qi, F Z / Qi, M / Qian, X / Raper, N / Ren, J / Morales Reveco, C / Rosero, R / Roskovec, B / Ruan, X C / Searles, M / Steiner, H / Sun, J L / Surukuchi, P T / Tmej, T / Treskov, K / Tse, W-H / Tull, C E / Tyra, M A / Varner, R L / Venegas-Vargas, D / Viren, B / Vorobel, V / Wang, C H / Wang, J / Wang, M / Wang, N Y / Wang, R G / Wang, W / Wang, X / Wang, Y / Wang, Y F / Wang, Z / Wang, Z M / Weatherly, P B / Wei, H Y / Wei, L H / Wen, L J / Whisnant, K / White, C / Wilhelmi, J / Wong, H L H / Woolverton, A / Worcester, E / Wu, D R / Wu, F L / Wu, Q / Wu, W J / Xia, D M / Xie, Z Q / Xing, Z Z / Xu, H K / Xu, J L / Xu, T / Xue, T / Yang, C G / Yang, L / Yang, Y Z / Yao, H F / Ye, M / Yeh, M / Young, B L / Yu, H Z / Yu, Z Y / Yue, B B / Zavadskyi, V / Zeng, S / Zeng, Y / Zhan, L / Zhang, C / Zhang, F Y / Zhang, H H / Zhang, J W / Zhang, Q M / Zhang, S Q / Zhang, X / Zhang, X T / Zhang, Y M / Zhang, Y X / Zhang, Y Y / Zhang, Z J / Zhang, Z P / Zhang, Z Y / Zhao, J / Zhao, R Z / Zhou, L / Zhuang, H L / Zou, J H

Physical review letters

2022 Volume 128, Issue 8, Page(s) 81801

Abstract: ... 239}Pu has been carried out by the Daya Bay and PROSPECT Collaborations. This Letter reports the level ... between the dominant ^{235}U and ^{239}Pu isotopes and improves the uncertainty of the ^{235}U spectral ... shape to about 3%. The ^{235}U and ^{239}Pu antineutrino energy spectra are unfolded from the jointly ...

Abstract	A joint determination of the reactor antineutrino spectra resulting from the fission of ^{235}U and ^{239}Pu has been carried out by the Daya Bay and PROSPECT Collaborations. This Letter reports the level of consistency of ^{235}U spectrum measurements from the two experiments and presents new results from a joint analysis of both data sets. The measurements are found to be consistent. The combined analysis reduces the degeneracy between the dominant ^{235}U and ^{239}Pu isotopes and improves the uncertainty of the ^{235}U spectral shape to about 3%. The ^{235}U and ^{239}Pu antineutrino energy spectra are unfolded from the jointly deconvolved reactor spectra using the Wiener-SVD unfolding method, providing a data-based reference for other reactor antineutrino experiments and other applications. This is the first measurement of the ^{235}U and ^{239}Pu spectra based on the combination of experiments at low- and highly enriched uranium reactors.
Language	English
Publishing date	2022-03-11
Publishing country	United States
Document type	Journal Article
ZDB-ID	208853-8
ISSN	1079-7114 ; 0031-9007
ISSN (online)	1079-7114
ISSN	0031-9007
DOI	10.1103/PhysRevLett.128.081801
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Article ; Online: Distinguishing raw pu-erh tea production regions through a combination of HS-SPME-GC-MS and machine learning algorithms

Xiong, Zhichao / Feng, Wanzhen / Xia, Dongzhou / Zhang, Jixin / Wei, Yuming / Li, Tiehan / Huang, Junlan / Wang, Yujie / Ning, Jingming

LWT. 2023 Aug., v. 185 p.115140-

2023

Abstract: ... attention. Tea tree varieties, processing processes and origins influence the quality and price of raw pu ...

Abstract	The authenticity of the geographical origin of agricultural products has received widespread attention. Tea tree varieties, processing processes and origins influence the quality and price of raw pu-erh tea (RPT). This study distinguished RPT from 10 different production areas through headspace solid-phase microextraction-gas chromatography-mass spectrometry (HS-SPME-GC-MS) combined with orthogonal partial least squares–discriminant analysis (OPLS-DA) model and machine learning algorithms. Among the thirty-five types of common volatiles identified, pentanal, heptanal, naphthalene, cedrol, and 2,6-di-tert-butylbenzoquinone were considered the key differential compounds distinguishing the 10 different production areas of the RPT samples through the screening of variable importance in projection values of the OPLS-DA and coefficient weights of the linear discriminant analysis function. Among them, heptanal and 2,6-di-tert-butylbenzoquinone had the highest content in West of Bingdao and the lowest content in Nannuoshan. The random forest algorithm achieved a discrimination accuracy of 98.4% based on the discrimination of five key compounds in 63 RPT samples. The random forest model was demonstrated to be reliable and valid by using receiver operating characteristic curves (area under the curve = 0.7603). The study results serve as a reference for the differentiation of 10 production areas of RPT.
Keywords	algorithms ; cedrol ; discriminant analysis ; headspace analysis ; mass spectrometry ; models ; naphthalene ; prices ; provenance ; tea ; trees ; Raw pu-erh tea ; Regional discrimination ; Volatile compounds ; GC-MS ; Machine learning
Language	English
Dates of publication	2023-08
Publishing place	Elsevier Ltd
Document type	Article ; Online
ZDB-ID	241369-3
ISSN	0460-1173 ; 0023-6438
ISSN	0460-1173 ; 0023-6438
DOI	10.1016/j.lwt.2023.115140
Database	NAL-Catalogue (AGRICOLA)

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Article ; Online: A wearable sweat electrochemical aptasensor based on the Ni–Co MOF nanosheet-decorated CNTs/PU film for monitoring of stress biomarker

Su, Tong / Mi, Ziyi / Xia, Youyuan / Jin, Dangqin / Xu, Qin / Hu, Xiaoya / Shuyun

Talanta. 2023 Aug., v. 260 p.124620-

2023

Abstract	Monitoring cortisol, a hormone released by the adrenal cortex in response to stress, is essential to evaluate the endocrine response to stress stimuli. While the current cortisol sensing methods require large laboratory settings, complex assay, and professional personnel. Herein, a novel flexible and wearable electrochemical aptasensor based on a Ni–Co metal-organic frameworks (MOF) nanosheet-decorated carbon nanotubes (CNTs)/polyurethane (PU) film is developed for rapid and reliable detection of cortisol in sweat. First, the CNTs/PU (CP) film was prepared by a modified wet spinning technology, and the CNTs/polyvinyl alcohol (PVA) solution was thermally deposited on the surface of CP film to form the highly flexible CNTs/PVA/CP (CCP) film with excellent conductivity. Then aminated Ni–Co MOF nanosheet prepared by a facile solvothermal method was conjugated with streptavidin and modified on the CCP film. Biofunctional MOF can effectively capture cortisol aptamer due to its excellent specific surface area. In addition, the MOF with peroxidase activity can catalytic oxidization of hydroquinone (HQ) by hydrogen peroxide (H₂O₂), which could amplify the peak current signal. The catalytic activity of Ni–Co MOF was substantially suppressed in the HQ/H₂O₂ system due to the formation of the aptamer-cortisol complex, which reduced the current signal, thereby realizing highly sensitive and selective detection of cortisol. The sensor has a linear range of 0.1–100 ng/mL and a detection limit of 0.032 ng/mL. Meanwhile, the sensor showed high accuracy for cortisol detection under mechanical deformation conditions. More importantly, the prepared MOF/CCP film based three-electrode was assembled with the polydimethylsiloxane (PDMS) substrate, and the sweat-cloth was used as the sweat collection channel to fabricate a wearable sensor patch for monitoring of cortisol in volunteers’ sweat in the morning and evening. This flexible and non-invasive sweat cortisol aptasensor shows great potential for quantitative stress monitoring and management.
Keywords	adrenal cortex ; aptasensors ; biomarkers ; carbon nanotubes ; catalytic activity ; cortisol ; deformation ; detection limit ; electrochemistry ; human resources ; hydrogen peroxide ; hydroquinone ; nanosheets ; oligonucleotides ; peroxidase ; polydimethylsiloxane ; polyvinyl alcohol ; streptavidin ; stress response ; surface area ; sweat ; Wearable electrochemical aptasensor ; Ni–Co metal-Organic framework ; Cortisol monitoring
Language	English
Dates of publication	2023-08
Publishing place	Elsevier B.V.
Document type	Article ; Online
ZDB-ID	1500969-5
ISSN	1873-3573 ; 0039-9140
ISSN (online)	1873-3573
ISSN	0039-9140
DOI	10.1016/j.talanta.2023.124620
Database	NAL-Catalogue (AGRICOLA)

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Article ; Online: Correction to Ripened Pu-erh Tea Extract Promotes Gut Microbiota Resilience against Dextran Sulfate Sodium Induced Colitis.

Huang, Yina / Yang, Qin / Mi, Xuan / Qiu, Liang / Tao, Xueying / Zhang, Zhihong / Xia, Jun / Wu, Qinglong / Wei, Hua

Journal of agricultural and food chemistry

2021 Volume 69, Issue 11, Page(s) 3559

Language	English
Publishing date	2021-03-11
Publishing country	United States
Document type	Published Erratum
ZDB-ID	241619-0
ISSN	1520-5118 ; 0021-8561
ISSN (online)	1520-5118
ISSN	0021-8561
DOI	10.1021/acs.jafc.1c01333
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