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  1. Article: Data science enabled discovery of a highly soluble 2,2'-bipyrimidine anolyte for application in a flow battery.

    Pancoast, Adam R / McCormack, Sara L / Galinat, Shelby / Walser-Kuntz, Ryan / Jett, Brianna M / Sanford, Melanie S / Sigman, Matthew S

    Chemical science

    2023  Volume 14, Issue 47, Page(s) 13734–13742

    Abstract: Development of non-aqueous redox flow batteries as a viable energy storage solution relies upon the identification of soluble charge carriers capable of storing large amounts of energy over extended time periods. A combination of metrics including number ...

    Abstract Development of non-aqueous redox flow batteries as a viable energy storage solution relies upon the identification of soluble charge carriers capable of storing large amounts of energy over extended time periods. A combination of metrics including number of electrons stored per molecule, redox potential, stability, and solubility of the charge carrier impact performance. In this context, we recently reported a 2,2'-bipyrimidine charge carrier that stores two electrons per molecule with reduction near -2.0 V
    Language English
    Publishing date 2023-11-02
    Publishing country England
    Document type Journal Article
    ZDB-ID 2559110-1
    ISSN 2041-6539 ; 2041-6520
    ISSN (online) 2041-6539
    ISSN 2041-6520
    DOI 10.1039/d3sc04084d
    Database MEDical Literature Analysis and Retrieval System OnLINE

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  2. Article ; Online: A Unified Approach to Couple Aromatic Heteronucleophiles to Azines and Pharmaceuticals.

    Anderson, Ryan G / Jett, Brianna M / McNally, Andrew

    Angewandte Chemie (International ed. in English)

    2018  Volume 57, Issue 38, Page(s) 12514–12518

    Abstract: Coupling aromatic heteronucleophiles to arenes is a common way to assemble drug-like molecules. Many methods operate via nucleophiles intercepting organometallic intermediates, via Pd-, Cu-, and Ni-catalysis, that facilitate carbon-heteroatom bond ... ...

    Abstract Coupling aromatic heteronucleophiles to arenes is a common way to assemble drug-like molecules. Many methods operate via nucleophiles intercepting organometallic intermediates, via Pd-, Cu-, and Ni-catalysis, that facilitate carbon-heteroatom bond formation and a variety of protocols. We present an alternative, unified strategy where phosphonium salts can replicate the behavior of organometallic intermediates. Under a narrow set of reaction conditions, a variety of aromatic heteronucleophile classes can be coupled to pyridines and diazines that are often problematic in metal-catalyzed couplings, such as where (pseudo)halide precursors are unavailable in complex structures with multiple polar functional groups.
    MeSH term(s) Carbon/chemistry ; Catalysis ; Copper/chemistry ; Heterocyclic Compounds/chemistry ; Nickel/chemistry ; Palladium/chemistry ; Pharmaceutical Preparations/chemistry ; Pyridines/chemistry
    Chemical Substances Heterocyclic Compounds ; Pharmaceutical Preparations ; Pyridines ; Palladium (5TWQ1V240M) ; Carbon (7440-44-0) ; Copper (789U1901C5) ; Nickel (7OV03QG267)
    Language English
    Publishing date 2018-08-27
    Publishing country Germany
    Document type Journal Article ; Research Support, N.I.H., Extramural ; Research Support, Non-U.S. Gov't
    ZDB-ID 2011836-3
    ISSN 1521-3773 ; 1433-7851
    ISSN (online) 1521-3773
    ISSN 1433-7851
    DOI 10.1002/anie.201807322
    Database MEDical Literature Analysis and Retrieval System OnLINE

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  3. Article: Selective formation of heteroaryl thioethers via a phosphonium ion coupling reaction.

    Anderson, Ryan G / Jett, Brianna M / McNally, Andrew

    Tetrahedron

    2017  Volume 74, Issue 25, Page(s) 3129–3136

    Abstract: Heteroaryl thioethers, comprised of pyridines and diazines, are an important class of compounds with relevance to medicinal chemistry. Metal-catalyzed cross-couplings and ... ...

    Abstract Heteroaryl thioethers, comprised of pyridines and diazines, are an important class of compounds with relevance to medicinal chemistry. Metal-catalyzed cross-couplings and S
    Language English
    Publishing date 2017-12-21
    Publishing country England
    Document type Journal Article
    ZDB-ID 204285-x
    ISSN 1464-5416 ; 0040-4020 ; 0563-2064
    ISSN (online) 1464-5416
    ISSN 0040-4020 ; 0563-2064
    DOI 10.1016/j.tet.2017.12.040
    Database MEDical Literature Analysis and Retrieval System OnLINE

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