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Article ; Online: Novel D-π-A hemicyanine dye as photoinitiators for in situ hydrogel formation and DLP printing.

Du, Yao / Zhang, Yating / Liu, Shitao / Zhang, Xiwang / Wang, Tao

2024

Abstract: The field of biofabrication imposes stringent requirements on the polymerization activity and biosafety of photopolymeric hydrogel systems. In this investigation, we designed and synthesized four hemicyanine dyes with a D-π-A structure specifically ... ...

Abstract	The field of biofabrication imposes stringent requirements on the polymerization activity and biosafety of photopolymeric hydrogel systems. In this investigation, we designed and synthesized four hemicyanine dyes with a D-π-A structure specifically tailored for biofabrication purposes. These novel dyes, incorporating carbazole (CZ), triphenylamine (TPA), anthracene (AN), and benzodithiophene (BDT) as electron donors, along with heterocyclic salt (IN) as electron acceptors, were prepared using a straightforward synthesis method. The absorption maxima of ANIN, CZIN, and TPAIN exceeded 500 nm, rendering them suitable co-initiators for the free radical photopolymerization of acrylates under green-red light exposure facilitated by light-emitting diodes (LEDs) and the co-initiator iodonium salt (ION). Notably, CZIN and TPAIN, due to their robust dye absorption and efficient electron transfer to ION, functioned as high-performance photosensitizers. Meanwhile, BDTIN, with its strong and broad absorption range (400-600 nm), enhanced the accuracy of visible light photopolymerization. These dyes exhibit characteristics such as facile synthesis, heightened photo stability, and non-toxicity and also demonstrate the ability to discern the alkalinity of a solution to some extent. Furthermore, we explored the application of these hemicyanine dyes in 3D printing, showing potential to enhance printing resolution in DLP 3D printing (digital light process 3D printing).
Language	English
Publishing date	2024-04-16
Publishing country	United States
Document type	Journal Article
ZDB-ID	123540-0
ISSN	1751-1097 ; 0031-8655
ISSN (online)	1751-1097
ISSN	0031-8655
DOI	10.1111/php.13947
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Article ; Online: Characteristics of the Seismic Signal Generated by Fragmental Rockfalls: Insight From Laboratory Experiments

Lin, Qiwen / Wang, Yufeng / Cheng, Qiangong / Deng, Kaifeng / Liu, Shitao / Li, Kun

Journal of Geophysical Research: Solid Earth. 2022 Nov., v. 127, no. 11 p.e2022JB025096-

2022

Abstract: Continuous seismic signals are proposed as a useful quantitative information source for the estimation of rockfall properties. However, few studies have examined the characteristics of the seismic signal of fragmentation‐related rockfalls. In this study, ...

Abstract	Continuous seismic signals are proposed as a useful quantitative information source for the estimation of rockfall properties. However, few studies have examined the characteristics of the seismic signal of fragmentation‐related rockfalls. In this study, a series of laboratory experiments designed with crushable analog blocks freefalling and impacting on a thin horizontal plate under different initial conditions (e.g., block volume, strength and fall height) were conducted. Strong correlations are observed between the rockfall properties and the seismic parameters when considering the rock fragmentation during impact. However, these relationships are observed only when the variation in potential energy spans over one order of magnitude, indicating that the application of seismic signals is limited by rockfall properties. In particular, the seismic energy calculated by the diffuse method is the most stable seismic parameter that is highly correlated with the potential energy of rockfalls. By compiling the available data of the seismic signals of both natural and experimental rockfalls from previous studies and our experiments, we found that the relationship between the seismic energy and the potential energy of rockfalls follows a power law model at all scales. The exponent of the power law function ranges from 1.11 to 1.69. Rock strength can significantly affect the seismic features, which are quantitatively discussed. Rock fragmentation acts as an intermediate variable, which is controlled by rockfall properties and consequently affects the corresponding seismic characteristics. Furthermore, rock fragmentation reduces the efficiency of the conversion of potential energy to seismic energy of rockfalls.
Keywords	geophysics ; information sources ; mathematical models ; potential energy ; research ; rockfalls
Language	English
Dates of publication	2022-11
Publishing place	John Wiley & Sons, Ltd
Document type	Article ; Online
Note	JOURNAL ARTICLE
ISSN	2169-9313
DOI	10.1029/2022JB025096
Database	NAL-Catalogue (AGRICOLA)

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Article ; Online: Novel Sulfonamide Derivatives Containing a Piperidine Moiety as New Bactericide Leads for Managing Plant Bacterial Diseases.

Xie, Jiao / Long, Zhou-Qing / Chen, Ai-Qun / Ding, Ying-Guo / Liu, Shi-Tao / Zhou, Xiang / Liu, Li-Wei / Yang, Song

International journal of molecular sciences

2023 Volume 24, Issue 6

Abstract: Plant bacterial diseases are an intractable problem due to the fact that phytopathogens have acquired strong resistances for traditional pesticides, resulting in restricting the quality and yield of agricultural products around the world. To develop new ... ...

Abstract	Plant bacterial diseases are an intractable problem due to the fact that phytopathogens have acquired strong resistances for traditional pesticides, resulting in restricting the quality and yield of agricultural products around the world. To develop new agrochemical alternatives, we prepared a novel series of sulfanilamide derivatives containing piperidine fragments and assessed their antibacterial potency. The bioassay results revealed that most molecules displayed excellent in vitro antibacterial potency towards
MeSH term(s)	Dihydropteroate Synthase ; Oxadiazoles/pharmacology ; Microbial Sensitivity Tests ; Oryza/microbiology ; Anti-Bacterial Agents/pharmacology ; Anti-Bacterial Agents/chemistry ; Sulfanilamide ; Xanthomonas ; Sulfonamides/pharmacology ; Piperidines/pharmacology ; Bacterial Infections ; Plant Diseases/prevention & control ; Plant Diseases/microbiology
Chemical Substances	bismerthiazol ; Dihydropteroate Synthase (EC 2.5.1.15) ; Oxadiazoles ; Anti-Bacterial Agents ; Sulfanilamide (21240MF57M) ; Sulfonamides ; Piperidines
Language	English
Publishing date	2023-03-20
Publishing country	Switzerland
Document type	Journal Article
ZDB-ID	2019364-6
ISSN	1422-0067 ; 1422-0067 ; 1661-6596
ISSN (online)	1422-0067
ISSN	1422-0067 ; 1661-6596
DOI	10.3390/ijms24065861
Database	MEDical Literature Analysis and Retrieval System OnLINE

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Article ; Online: Recent progress and outlooks in rhodamine-based fluorescent probes for detection and imaging of reactive oxygen, nitrogen, and sulfur species.

Yang, Ping / Tang, A-Ling / Tan, Shuai / Wang, Guang-Ye / Huang, Hou-Yun / Niu, Wei / Liu, Shi-Tao / Ge, Mei-Hong / Yang, Lin-Lin / Gao, Feng / Zhou, Xiang / Liu, Li-Wei / Yang, Song

Talanta

2024 Volume 274, Page(s) 126004

Abstract: Reactive oxygen species (ROS), reactive nitrogen species (RNS), and reactive sulfur species (RSS) serve as vital mediators essential for preserving intracellular redox homeostasis within the human body, thereby possessing significant implications across ... ...

Abstract	Reactive oxygen species (ROS), reactive nitrogen species (RNS), and reactive sulfur species (RSS) serve as vital mediators essential for preserving intracellular redox homeostasis within the human body, thereby possessing significant implications across physiological and pathological domains. Nevertheless, deviations from normal levels of ROS, RNS, and RSS disturb redox homeostasis, leading to detrimental consequences that compromise bodily integrity. This disruption is closely linked to the onset of various human diseases, thereby posing a substantial threat to human health and survival. Small-molecule fluorescent probes exhibit considerable potential as analytical instruments for the monitoring of ROS, RNS, and RSS due to their exceptional sensitivity and selectivity, operational simplicity, non-invasiveness, localization capabilities, and ability to facilitate in situ optical signal generation for real-time dynamic analyte monitoring. Due to their distinctive transition from their spirocyclic form (non-fluorescent) to their ring-opened form (fluorescent), along with their exceptional light stability, broad wavelength range, high fluorescence quantum yield, and high extinction coefficient, rhodamine fluorophores have been extensively employed in the development of fluorescent probes. This review primarily concentrates on the investigation of fluorescent probes utilizing rhodamine dyes for ROS, RNS, and RSS detection from the perspective of different response groups since 2016. The scope of this review encompasses the design of probe structures, elucidation of response mechanisms, and exploration of biological applications.
MeSH term(s)	Fluorescent Dyes/chemistry ; Rhodamines/chemistry ; Reactive Nitrogen Species/analysis ; Humans ; Reactive Oxygen Species/metabolism ; Reactive Oxygen Species/analysis ; Optical Imaging ; Animals ; Sulfur/chemistry ; Sulfur/analysis
Chemical Substances	Fluorescent Dyes ; Rhodamines ; Reactive Nitrogen Species ; Reactive Oxygen Species ; Sulfur (70FD1KFU70)
Language	English
Publishing date	2024-04-01
Publishing country	Netherlands
Document type	Journal Article ; Review
ZDB-ID	1500969-5
ISSN	1873-3573 ; 0039-9140
ISSN (online)	1873-3573
ISSN	0039-9140
DOI	10.1016/j.talanta.2024.126004
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Article ; Online: Application of dental pulp stem cells in oral maxillofacial tissue engineering.

Liu, Peng / Zhang, Yingxin / Ma, Yujie / Tan, Shuang / Ren, Bingyi / Liu, Shitao / Dai, HuanYan / Xu, Zhimin

International journal of medical sciences

2022 Volume 19, Issue 2, Page(s) 310–320

Abstract: In the maxillofacial area, soft and hard tissue abnormalities are caused by trauma, tumors, infection, and other causes that expose the maxillofacial region to the surface of the human body. Patients' normal physiological function and appearance are ... ...

Abstract	In the maxillofacial area, soft and hard tissue abnormalities are caused by trauma, tumors, infection, and other causes that expose the maxillofacial region to the surface of the human body. Patients' normal physiological function and appearance are interfered with, and their mental health is adversely impacted, reducing their overall life quality. The pursuit of appropriate medical treatments to correct these abnormalities is thus vital. Autologous stem cell regeneration technology mainly focused on tissues has lately emerged as a significant problem in the medical community. Because of the capacity of dental pulp stem cells (DPSCs) to self-renew, the use of DPSCs from the human pulp tissues of deciduous teeth or permanent teeth has gained popularity among scientists as a stem cell-based therapy option. Aside from that, they are simple to extract and have minimal immunogenicity. As a result, bone tissue engineering may be a critical component in treating maxillofacial and periodontal bone abnormalities. DPSCs activity in maxillofacial and periodontal tissue-engineered bone tissue was investigated in this research.
MeSH term(s)	Dental Pulp/cytology ; Humans ; Stem Cell Transplantation ; Stem Cells/cytology ; Surgery, Oral/methods ; Tissue Engineering/methods
Language	English
Publishing date	2022-01-11
Publishing country	Australia
Document type	Journal Article ; Review
ZDB-ID	2151424-0
ISSN	1449-1907 ; 1449-1907
ISSN (online)	1449-1907
ISSN	1449-1907
DOI	10.7150/ijms.68494
Database	MEDical Literature Analysis and Retrieval System OnLINE

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Article ; Online: Discovery of novel rost-4-ene derivatives as potential plant activators for preventing phytopathogenic bacterial infection: Design, synthesis and biological studies.

Wang, Fang / Liu, Hong-Wu / Zhang, Ling / Liu, Shi-Tao / Zhang, Jun-Rong / Zhou, Xiang / Wang, Pei-Yi / Yang, Song

Pest management science

2022 Volume 78, Issue 8, Page(s) 3404–3415

Abstract: Background: Gradually aggravated disease caused by phytopathogenic bacteria severely restricts food security and crop yield, and few pesticides can relieve this severe situation. Thus, development and excavation of new agrochemicals with high ... ...

Abstract	Background: Gradually aggravated disease caused by phytopathogenic bacteria severely restricts food security and crop yield, and few pesticides can relieve this severe situation. Thus, development and excavation of new agrochemicals with high bioactivity and novel action mechanism may be a feasible strategy to control intractable bacterial diseases. As a privileged molecular framework, steroid molecules exhibit diversiform bioactivities. Herein, a series of novel androst-4-ene derivatives were designed, synthesised and investigated for their antibacterial behaviour to excavate novel agrochemicals on the base of steroid molecules. Results: Bioassay results indicated that target compounds displayed high bioactivities toward three destructive phytopathogenic bacteria, including Xanthomonas oryzae pv. oryzae (Xoo), Xanthomonas axonopodis pv. citri (Xac) and Pseudomonas syringae pv. actinidiae (Psa). Compound III Conclusion: Given these profiles of target compounds, we highlight a new strategy for controlling intractable plant bacterial diseases by inducing plant resistance and targeting the bacterial cell membrane. © 2022 Society of Chemical Industry.
MeSH term(s)	Agrochemicals ; Anti-Bacterial Agents ; Bacterial Infections ; Microbial Sensitivity Tests ; Oryza ; Oxadiazoles/chemistry ; Plant Diseases/prevention & control ; Xanthomonas
Chemical Substances	Agrochemicals ; Anti-Bacterial Agents ; Oxadiazoles
Language	English
Publishing date	2022-05-27
Publishing country	England
Document type	Journal Article
ZDB-ID	2001705-4
ISSN	1526-4998 ; 1526-498X
ISSN (online)	1526-4998
ISSN	1526-498X
DOI	10.1002/ps.6981
Database	MEDical Literature Analysis and Retrieval System OnLINE

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Article: Discovery of novel rost‐4‐ene derivatives as potential plant activators for preventing phytopathogenic bacterial infection: Design, synthesis and biological studies

Wang, Fang / Liu, Hong‐Wu / Zhang, Ling / Liu, Shi‐Tao / Zhang, Jun‐Rong / Zhou, Xiang / Wang, Pei‐Yi / Yang, Song

Pest management science. 2022 Aug., v. 78, no. 8

2022

Abstract: BACKGROUND: Gradually aggravated disease caused by phytopathogenic bacteria severely restricts food security and crop yield, and few pesticides can relieve this severe situation. Thus, development and excavation of new agrochemicals with high bioactivity ...

Abstract	BACKGROUND: Gradually aggravated disease caused by phytopathogenic bacteria severely restricts food security and crop yield, and few pesticides can relieve this severe situation. Thus, development and excavation of new agrochemicals with high bioactivity and novel action mechanism may be a feasible strategy to control intractable bacterial diseases. As a privileged molecular framework, steroid molecules exhibit diversiform bioactivities. Herein, a series of novel androst‐4‐ene derivatives were designed, synthesised and investigated for their antibacterial behaviour to excavate novel agrochemicals on the base of steroid molecules. RESULTS: Bioassay results indicated that target compounds displayed high bioactivities toward three destructive phytopathogenic bacteria, including Xanthomonas oryzae pv. oryzae (Xoo), Xanthomonas axonopodis pv. citri (Xac) and Pseudomonas syringae pv. actinidiae (Psa). Compound III₁₉ displayed excellent in vitro antibacterial profiling (EC₅₀ = 2.37 mg L⁻¹ towards Xoo, EC₅₀ = 2.10 mg L⁻¹ towards Xac, EC₅₀ = 9.50 mg L⁻¹ towards Psa). Furthermore, compound III₁₉ showed outstanding in vivo protective activities, with values of 81.81% and 58.75% towards kiwifruit bacterial canker and rice bacterial leaf blight, respectively. Analysis of the antibacterial mechanism disclosed that compound III₁₉ enhanced host defence enzyme activities superoxide dismutase (SOD), peroxidase (POD), phenylalanine ammonia lyase (PAL), polyphenol oxidase (PPO), and catalase (CAT) and increased the salicylate synthase content to induce host resistance. In addition, compound III₁₉ increased the membrane permeability, destroyed the cell membrane and killed the bacteria. CONCLUSION: Given these profiles of target compounds, we highlight a new strategy for controlling intractable plant bacterial diseases by inducing plant resistance and targeting the bacterial cell membrane. © 2022 Society of Chemical Industry.
Keywords	Pseudomonas syringae pv. actinidiae ; Xanthomonas axonopodis pv. citri ; Xanthomonas oryzae pv. oryzae ; agrochemicals ; antibacterial properties ; bacterial canker ; bacterial infections ; bioassays ; catalase ; catechol oxidase ; cell membranes ; crop yield ; food security ; kiwifruit ; leaf blight ; membrane permeability ; peroxidase ; phenylalanine ammonia-lyase ; superoxide dismutase
Language	English
Dates of publication	2022-08
Size	p. 3404-3415.
Publishing place	John Wiley & Sons, Ltd.
Document type	Article
Note	JOURNAL ARTICLE
ZDB-ID	2001705-4
ISSN	1526-4998 ; 1526-498X
ISSN (online)	1526-4998
ISSN	1526-498X
DOI	10.1002/ps.6981
Database	NAL-Catalogue (AGRICOLA)

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Article ; Online: Rhodamine-based fluorescent sensors for the rapid and selective off-on detection of salicylic acid and their use in plant cell imaging.

Chen, Jie-Ying / Yang, Ping / Huang, Hou-Yun / Tang, A-Ling / Ge, Mei-Hong / Niu, Wei / Liu, Shi-Tao / Tan, Shuai / Ma, Wen-Jing / Zhou, Xiang / Liu, Li-Wei / Yang, Song

Organic & biomolecular chemistry

2023 Volume 21, Issue 33, Page(s) 6783–6788

Abstract: Salicylic acid (SA) is a key hormone that regulates plant growth and immunity, and understanding the physiologic processes induced by SA enables the development of highly pathogen-resistant crops. Here, we report the synthesis of three new SA-sensors (R1- ...

Abstract	Salicylic acid (SA) is a key hormone that regulates plant growth and immunity, and understanding the physiologic processes induced by SA enables the development of highly pathogen-resistant crops. Here, we report the synthesis of three new SA-sensors (R1-R3) from hydroxyphenol derivatives of a rhodamine-acylhydrazone scaffold and their characterization by NMR and HRMS. Spectroscopic analyses revealed that structural variations in R1-R3 resulted in sensors with different sensitivities for SA. Sensor R2 (with the 3-hydroxyphenyl modification) outperformed R1 (2-hydroxyphenyl) and R3 (4-hydroxyphenyl). The SA-detection limit of R2 is 0.9 μM with an ultra-fast response time (<60 s). In addition, their plant imaging indicated that designed sensor R2 is useful for the further study of SA biology and the discovery and development of new inducers of plant immunity.
MeSH term(s)	Rhodamines/chemistry ; Salicylic Acid/analysis ; Salicylic Acid/chemistry ; Plant Cells/chemistry ; Coloring Agents ; Plants
Chemical Substances	Rhodamines ; Salicylic Acid (O414PZ4LPZ) ; Coloring Agents
Language	English
Publishing date	2023-08-23
Publishing country	England
Document type	Journal Article ; Research Support, Non-U.S. Gov't
ZDB-ID	2097583-1
ISSN	1477-0539 ; 1477-0520
ISSN (online)	1477-0539
ISSN	1477-0520
DOI	10.1039/d3ob01052j
Database	MEDical Literature Analysis and Retrieval System OnLINE

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Article ; Online: Substituent-controlled chemoselective synthesis of multi-substituted pyridones via a one-pot three-component cascade reaction.

Liu, Shitao / Li, Jisen / Lin, Junjie / Liu, Fujun / Liu, Teng / Huang, Chao

Organic & biomolecular chemistry

2020 Volume 18, Issue 6, Page(s) 1130–1134

Abstract: An efficient and concise one-pot strategy for the synthesis of multisubstituted pyridones via a one-pot three-component cascade reaction catalyzed by ... ...

Abstract	An efficient and concise one-pot strategy for the synthesis of multisubstituted pyridones via a one-pot three-component cascade reaction catalyzed by Cs
Language	English
Publishing date	2020-01-20
Publishing country	England
Document type	Journal Article ; Research Support, Non-U.S. Gov't
ZDB-ID	2097583-1
ISSN	1477-0539 ; 1477-0520
ISSN (online)	1477-0539
ISSN	1477-0520
DOI	10.1039/c9ob02456e
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Article ; Online: Highly Selective and Rapid "Turn-On" Fluorogenic Chemosensor for Detection of Salicylic Acid in Plants and Food Samples.

Chen, Jie-Ying / Tang, A-Ling / Yang, Ping / Yang, Lin-Lin / Tan, Shuai / Ma, Wen-Jing / Liu, Shi-Tao / Huang, Hou-Yun / Zhou, Xiang / Liu, Li-Wei / Yang, Song

ACS sensors

2023 Volume 8, Issue 11, Page(s) 4020–4030

Abstract: Salicylic acid (SA) is one of the chemical molecules, involved in plant growth and immunity, thereby contributing to the control of pests and pathogens, and even applied in fruit and vegetable preservation. However, only a few tools have ever been ... ...

Abstract	Salicylic acid (SA) is one of the chemical molecules, involved in plant growth and immunity, thereby contributing to the control of pests and pathogens, and even applied in fruit and vegetable preservation. However, only a few tools have ever been designed or executed to understand the physiological processes induced by SA or its function in plant immunity and residue detection in food. Hence, three Rh6G-based fluorogenic chemosensors were synthesized to detect phytohormone SA based on the "OFF-ON" mechanism. The probes showed high selectivity, ultrafast response time (<60 s), and nanomolar detection limit for SA. Moreover, the probe possessed outstanding profiling that can be successfully used for SA imaging of callus and plants. Furthermore, the fluorescence pattern indicated that SA could occur in the distal transport in plants. These remarkable results contribute to improving our understanding of the multiple physiological and pathological processes involved in SA for plant disease diagnosis and for the development of immune activators. In addition, SA detection in some agricultural products used probes to extend the practical application because its use is prohibited in some countries and is harmful to SA-sensitized persons. Interestingly, the as-obtained test paper displayed that SA could be imaged by ultraviolet (UV) and was directly visible to the naked eye. Given the above outcomes, these probes could be used to monitor SA in vitro and in vivo, including, but not limited to, plant biology, food residue detection, and sewage detection.
MeSH term(s)	Salicylic Acid/chemistry ; Salicylic Acid/pharmacology ; Plant Growth Regulators/chemistry
Chemical Substances	Salicylic Acid (O414PZ4LPZ) ; Plant Growth Regulators
Language	English
Publishing date	2023-11-02
Publishing country	United States
Document type	Journal Article ; Research Support, Non-U.S. Gov't
ISSN	2379-3694
ISSN (online)	2379-3694
DOI	10.1021/acssensors.3c00159
Database	MEDical Literature Analysis and Retrieval System OnLINE

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