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Book ; Online ; E-Book: Green synthesized iron-based nanomaterials

Mondal, Piyal / Purkait, Mihir Kumar

applications and potential risks

(Emerging Materials and Technologies)

2023

Author's details	Piyal Mondal, Mihir Kumar Purkait
Series title	Emerging Materials and Technologies
Keywords	Nanostructured materials/Environmental aspects
Subject code	780
Language	English
Size	1 online resource (142 pages)
Publisher	CRC Press
Publishing place	Boca Raton, Florida ; Abingdon, Oxon
Document type	Book ; Online ; E-Book
Remark	Zugriff für angemeldete ZB MED-Nutzerinnen und -Nutzer
ISBN	1-00-324363-0 ; 1-003-24363-0 ; 1-000-64516-9 ; 1-03-215326-1 ; 978-1-00-324363-2 ; 978-1-003-24363-2 ; 978-1-000-64516-3 ; 978-1-03-215326-1
Database	ZB MED Catalogue: Medicine, Health, Nutrition, Environment, Agriculture

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Book ; Online ; E-Book: pH responsive membranes

Singh, Randeep / Mondal, Piyal / Purkait, Mihir K.

biomedical applications

2022

Abstract: The book provides an application-oriented approach for pH responsive membranes, a type of stimuli responsive membrane and their applications in the biomedical field including initial development and recent use. It explains types, modes, and modification ...

Author's details	Randeep Singh, Piyal Mondal, Mihir Kumar Purkait
Abstract	"The book provides an application-oriented approach for pH responsive membranes, a type of stimuli responsive membrane and their applications in the biomedical field including initial development and recent use. It explains types, modes, and modification methods of membranes along with membrane usage in applications such as drug delivery, haemodialysis, chemical sensing and so forth. The potential research carried out in the area as well as future scope is discussed, that provides better insights to the readers about the subject ranging from the basics to the advanced level of the topic"--
Keywords	Membranes (Biology) ; Hydrogen-ion concentration ; Chemistry, Physical and theoretical
Subject code	574.875
Language	English
Size	1 online resource (105 pages)
Publisher	CRC Press
Publishing place	Boca Raton, Florida ; London ; New York
Document type	Book ; Online ; E-Book
Remark	Zugriff für angemeldete ZB MED-Nutzerinnen und -Nutzer
ISBN	1-00-320101-6 ; 1-000-52070-6 ; 1-003-20101-6 ; 1-03-206167-7 ; 978-1-00-320101-4 ; 978-1-000-52070-5 ; 978-1-003-20101-4 ; 978-1-03-206167-2
Database	ZB MED Catalogue: Medicine, Health, Nutrition, Environment, Agriculture

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Article ; Online: Preparation and characterization of novel green synthesized iron-aluminum nanocomposite and studying its efficiency in fluoride removal.

Mondal, Piyal / Purkait, Mihir Kumar

Chemosphere

2019 Volume 235, Page(s) 391–402

Abstract: A novel green synthesized iron-aluminum nanocomposite was prepared and characterized by FESEM, FTIR, EDX, XRD, BET, DSC and TGA analysis. The clove extract acting as both reducing and surface coating agent was optimized based on its maximum total ... ...

Abstract	A novel green synthesized iron-aluminum nanocomposite was prepared and characterized by FESEM, FTIR, EDX, XRD, BET, DSC and TGA analysis. The clove extract acting as both reducing and surface coating agent was optimized based on its maximum total flavonoid content (TFC) and total polyphenolic content (TPC). Fluoride adsorption studies was performed at 298K, 303K and 313K within the range of 10-40 mg/L fluoride solution for kinetic and isotherm studies. Maximum adsorption capacity of 42.95 mg/g was obtained for 0.25 g/L adsorbent dosage. Moreover fluoride adsorption obeyed pseudo second order kinetic model whereas the process was multistage diffusion controlled. Langmuir isotherm model best fitted the equilibrium data with monolayer adsorption capacities of 25.09, 26.08 and 28.07 mg/g at 298, 303 and 313K respectively. The findings confirmed that the fluoride adsorption process followed ion exchange mechanism with the surface hydroxyl groups. The prepared nanocomposite was utilized for treating fluoride contaminated water samples from north-east regions of India which showed efficient removal percentage.
MeSH term(s)	Adsorption ; Aluminum ; Diffusion ; Fluorides/analysis ; Fluorides/chemistry ; Hydrogen-Ion Concentration ; India ; Iron ; Kinetics ; Nanocomposites/chemistry ; Thermodynamics ; Water Pollutants, Chemical/analysis ; Water Pollutants, Chemical/chemistry ; Water Purification/methods
Chemical Substances	Water Pollutants, Chemical ; Aluminum (CPD4NFA903) ; Iron (E1UOL152H7) ; Fluorides (Q80VPU408O)
Language	English
Publishing date	2019-06-25
Publishing country	England
Document type	Journal Article
ZDB-ID	120089-6
ISSN	1879-1298 ; 0045-6535 ; 0366-7111
ISSN (online)	1879-1298
ISSN	0045-6535 ; 0366-7111
DOI	10.1016/j.chemosphere.2019.06.189
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Article ; Online: Preparation and characterization of novel green synthesized iron–aluminum nanocomposite and studying its efficiency in fluoride removal

Mondal, Piyal / Purkait, Mihir K.

Chemosphere. 2019 Nov., v. 235 p.391-402

2019

Abstract	A novel green synthesized iron-aluminum nanocomposite was prepared and characterized by FESEM, FTIR, EDX, XRD, BET, DSC and TGA analysis. The clove extract acting as both reducing and surface coating agent was optimized based on its maximum total flavonoid content (TFC) and total polyphenolic content (TPC). Fluoride adsorption studies was performed at 298K, 303K and 313K within the range of 10–40 mg/L fluoride solution for kinetic and isotherm studies. Maximum adsorption capacity of 42.95 mg/g was obtained for 0.25 g/L adsorbent dosage. Moreover fluoride adsorption obeyed pseudo second order kinetic model whereas the process was multistage diffusion controlled. Langmuir isotherm model best fitted the equilibrium data with monolayer adsorption capacities of 25.09, 26.08 and 28.07 mg/g at 298, 303 and 313K respectively. The findings confirmed that the fluoride adsorption process followed ion exchange mechanism with the surface hydroxyl groups. The prepared nanocomposite was utilized for treating fluoride contaminated water samples from north-east regions of India which showed efficient removal percentage.
Keywords	Fourier transform infrared spectroscopy ; X-ray diffraction ; adsorbents ; adsorption ; cloves ; coatings ; differential scanning calorimetry ; energy-dispersive X-ray analysis ; flavonoids ; fluorides ; ion exchange ; kinetics ; models ; moieties ; nanocomposites ; scanning electron microscopy ; sorption isotherms ; thermogravimetry ; water pollution ; India ; Fe-Al nanocomposite ; Green synthesis ; Adsorption ; Fluoride removal ; Ion exchange
Language	English
Dates of publication	2019-11
Size	p. 391-402.
Publishing place	Elsevier Ltd
Document type	Article ; Online
ZDB-ID	120089-6
ISSN	1879-1298 ; 0045-6535 ; 0366-7111
ISSN (online)	1879-1298
ISSN	0045-6535 ; 0366-7111
DOI	10.1016/j.chemosphere.2019.06.189
Database	NAL-Catalogue (AGRICOLA)

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Article ; Online: Green synthesis and environmental application of iron-based nanomaterials and nanocomposite: A review

Mondal, Piyal / Anweshan, A. / Purkait, Mihir K.

Chemosphere. 2020 Nov., v. 259 p.127509-

2020

Abstract: Green chemistry has been proven to be an efficient route for nanoparticle synthesis. Plant extract based green synthesis of various nanoparticles is extensively studied since the last decade. This paper “Green synthesis and environmental application of ... ...

Abstract	Green chemistry has been proven to be an efficient route for nanoparticle synthesis. Plant extract based green synthesis of various nanoparticles is extensively studied since the last decade. This paper “Green synthesis and environmental application of Iron-based nanomaterials and nanocomposite: A review” unveils all the possible greener techniques for the synthesis of iron-based nanoparticles and nanocomposites. The use of different plant sources, microorganisms, and various biocompatible green reagents such as biopolymers, cellulose, haemoglobin, and glucose for the synthesis of iron nanoparticles reported in the last decade are summarized. The microwave method, along with hydrothermal synthesis due to their lower energy consumption are also been referred to as a green route. Apart from different plant parts, waste leaves and roots used for the synthesis of iron nanoparticles are extensively briefed here. This review is thus compact in nature which covers all the broad areas of green synthesis of iron nanoparticles (NPs) and iron-based nanocomposites. Detailed discussion on environmental applications of the various green synthesized iron NPs and their composites with performance efficiency is provided in this review article. The advantages of bimetallic iron-based nanocomposites over iron NPs in various environmental applications are discussed in detail. The hazards and toxic properties of green synthesized iron-based NPs are compared with those obtained from chemical methods. The prospects and challenges section of this article provides a vivid outlook of adapting such useful technique into a more versatile process with certain inclusions which may encourage and provide a new direction to future research.
Keywords	biopolymers ; cellulose ; energy ; glucose ; green chemistry ; hemoglobin ; iron ; leaves ; methodology ; microorganisms ; nanocomposites ; nanoparticles ; paper ; plant extracts ; research ; roots ; synthesis ; toxicity ; wastes ; Environmental application ; Green synthesis ; Iron nanoparticles ; Iron nanocomposites ; Toxic effects
Language	English
Dates of publication	2020-11
Publishing place	Elsevier Ltd
Document type	Article ; Online
Note	NAL-light
ZDB-ID	120089-6
ISSN	1879-1298 ; 0045-6535 ; 0366-7111
ISSN (online)	1879-1298
ISSN	0045-6535 ; 0366-7111
DOI	10.1016/j.chemosphere.2020.127509
Database	NAL-Catalogue (AGRICOLA)

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Article ; Online: Green synthesized iron nanoparticles supported on pH responsive polymeric membrane for nitrobenzene reduction and fluoride rejection study: Optimization approach

Mondal, Piyal / Purkait, Mihir K.

Journal of cleaner production. 2018 Jan. 01, v. 170 p.1111-1123

2018

Abstract: Iron nanoparticles (NPs) were prepared via Clove extract mediated green synthesis. Iron NPs were immobilized in flat asymmetric polymeric pH responsive PVDF-co-HFP membranes prepared by blending of Polyethylene glycol methyl ether (PEGME)(Mw = 5000 g/mol) ...

Abstract	Iron nanoparticles (NPs) were prepared via Clove extract mediated green synthesis. Iron NPs were immobilized in flat asymmetric polymeric pH responsive PVDF-co-HFP membranes prepared by blending of Polyethylene glycol methyl ether (PEGME)(Mw = 5000 g/mol) and Humic acid (HA). Iron NPs dispersed in pH responsive polymeric membrane in different weight percentage (0.01, 0.1 and 1) imparted catalytic effect in reducing nitrobenzene to aniline as well as enhanced fluoride rejection by dead end filtration experiment. Both the process of NB reduction and fluoride rejection was dependent on pH responsiveness of the membrane. High performance liquid chromatography (HPLC) analysed formation of aniline and nitrobenzene at different ultra-filtration time. Aniline formation of 15 ppm was found to be highest at pH3 and lowest of 12.8 ppm at pH7 for 0.01 wt% iron NPs impregnated membrane at end of 50 min. Aniline formation increased for pH12 than pH7 due to pH responsiveness. Fluoride rejection was studied on optimized wt% of iron NPs from NB reduction experiments with different pH of fluoride solutions. In order to maximize the Aniline formation and Nitrobenzene reduction, the variables (time, pH and wt% of NPs) was optimized using Design expert software 9.0 TRIAL through ANOVA (analysis of variance) using the combination of response surface methodology (RSM) and central composite design (CCD). The optimization study showed negligible error with experimentally obtained values at optimized conditions for maximizing NB reduction (error 3.37%) and aniline formation (error 3.93%).
Keywords	analysis of variance ; aniline ; cloves ; computer software ; filtration ; fluorides ; high performance liquid chromatography ; humic acids ; iron ; mixing ; nanoparticles ; pH ; polyethylene glycol ; response surface methodology ; Zero valent iron nanoparticle ; Polymeric pH responsive membrane support ; Nitrobenzene reduction ; Fluoride rejection ; Response surface methodology
Language	English
Dates of publication	2018-0101
Size	p. 1111-1123.
Publishing place	Elsevier Ltd
Document type	Article ; Online
ISSN	0959-6526
DOI	10.1016/j.jclepro.2017.09.222
Database	NAL-Catalogue (AGRICOLA)

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Article ; Online: Green synthesis and environmental application of iron-based nanomaterials and nanocomposite: A review.

Mondal, Piyal / Anweshan, A / Purkait, Mihir Kumar

Chemosphere

2020 Volume 259, Page(s) 127509

Abstract: Green chemistry has been proven to be an efficient route for nanoparticle synthesis. Plant extract based green synthesis of various nanoparticles is extensively studied since the last decade. This paper "Green synthesis and environmental application of ... ...

Abstract	Green chemistry has been proven to be an efficient route for nanoparticle synthesis. Plant extract based green synthesis of various nanoparticles is extensively studied since the last decade. This paper "Green synthesis and environmental application of Iron-based nanomaterials and nanocomposite: A review" unveils all the possible greener techniques for the synthesis of iron-based nanoparticles and nanocomposites. The use of different plant sources, microorganisms, and various biocompatible green reagents such as biopolymers, cellulose, haemoglobin, and glucose for the synthesis of iron nanoparticles reported in the last decade are summarized. The microwave method, along with hydrothermal synthesis due to their lower energy consumption are also been referred to as a green route. Apart from different plant parts, waste leaves and roots used for the synthesis of iron nanoparticles are extensively briefed here. This review is thus compact in nature which covers all the broad areas of green synthesis of iron nanoparticles (NPs) and iron-based nanocomposites. Detailed discussion on environmental applications of the various green synthesized iron NPs and their composites with performance efficiency is provided in this review article. The advantages of bimetallic iron-based nanocomposites over iron NPs in various environmental applications are discussed in detail. The hazards and toxic properties of green synthesized iron-based NPs are compared with those obtained from chemical methods. The prospects and challenges section of this article provides a vivid outlook of adapting such useful technique into a more versatile process with certain inclusions which may encourage and provide a new direction to future research.
MeSH term(s)	Green Chemistry Technology/methods ; Green Chemistry Technology/standards ; Iron/chemistry ; Metal Nanoparticles/chemistry ; Microwaves ; Nanocomposites/chemistry ; Plant Extracts/chemistry
Chemical Substances	Plant Extracts ; Iron (E1UOL152H7)
Language	English
Publishing date	2020-06-28
Publishing country	England
Document type	Journal Article ; Review
ZDB-ID	120089-6
ISSN	1879-1298 ; 0045-6535 ; 0366-7111
ISSN (online)	1879-1298
ISSN	0045-6535 ; 0366-7111
DOI	10.1016/j.chemosphere.2020.127509
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Article: Integrated ozonation assisted electrocoagulation process for the removal of cyanide from steel industry wastewater

Das, Pranjal P / Anweshan / Mondal, Piyal / Sinha, A / Biswas, P / Sarkar, S / Purkait, M.K

Chemosphere. 2021 Jan., v. 263

2021

Abstract: This work focuses on the removal of cyanide, chemical oxygen demand (COD), biological oxygen demand (BOD), and chloride from biological oxidation treated (BOT) effluent of the steel industry by integrated ozonation assisted electrocoagulation method. The ...

Abstract	This work focuses on the removal of cyanide, chemical oxygen demand (COD), biological oxygen demand (BOD), and chloride from biological oxidation treated (BOT) effluent of the steel industry by integrated ozonation assisted electrocoagulation method. The removal efficiency of the pollutants was found to be inefficient when the electrocoagulation or ozonation process was performed separately. However, a combination of ozonation and electrocoagulation gives a highly satisfactory result. Such an integrated approach for the treatment of BOT effluent has not been previously investigated. The effects of operating variables viz. ozone generation rate, current density, and analysis time on pollutant removal were primarily analyzed for the hybrid process. The experimental operating condition was optimized and was seen that ozone generation rate of 1.33 mg s⁻¹, ozonation time of 40 min, a current density of 100 A m⁻², and electrolysis time of 30 min were sufficient for reducing the pollutant concentration below its permissible limits. The removal efficiencies of the combined process at optimum conditions were 99.8%, 94.7%, 95%, and 46.5% for cyanide, COD, BOD, and chloride ions, respectively. A kinetic study was performed for the degradation of the pollutants during ozonation. The pseudo-first-order kinetic model was found to be best suited for the analysis with the highest R² value of 0.99 for cyanide, COD, BOD, and chloride, respectively. The mass transfer study conducted further showed that the volumetric mass transfer coefficient, Kₗa, was increased with that of the ozone generation rate. Cost estimation of the hybrid process was done and compared with that of the other reported integrated process.
Keywords	biochemical oxygen demand ; chemical oxygen demand ; chlorides ; cyanides ; electrocoagulation ; electrolysis ; industrial wastewater ; industry ; kinetics ; mass transfer ; oxidation ; ozonation ; ozone ; pollutants ; pollution control ; steel
Language	English
Dates of publication	2021-01
Publishing place	Elsevier Ltd
Document type	Article
Note	NAL-light
ZDB-ID	120089-6
ISSN	1879-1298 ; 0045-6535 ; 0366-7111
ISSN (online)	1879-1298
ISSN	0045-6535 ; 0366-7111
DOI	10.1016/j.chemosphere.2020.128370
Database	NAL-Catalogue (AGRICOLA)

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Article ; Online: Integrated ozonation assisted electrocoagulation process for the removal of cyanide from steel industry wastewater.

Das, Pranjal P / Anweshan / Mondal, Piyal / Sinha, A / Biswas, P / Sarkar, S / Purkait, M K

Chemosphere

2020 Volume 263, Page(s) 128370

Abstract	This work focuses on the removal of cyanide, chemical oxygen demand (COD), biological oxygen demand (BOD), and chloride from biological oxidation treated (BOT) effluent of the steel industry by integrated ozonation assisted electrocoagulation method. The removal efficiency of the pollutants was found to be inefficient when the electrocoagulation or ozonation process was performed separately. However, a combination of ozonation and electrocoagulation gives a highly satisfactory result. Such an integrated approach for the treatment of BOT effluent has not been previously investigated. The effects of operating variables viz. ozone generation rate, current density, and analysis time on pollutant removal were primarily analyzed for the hybrid process. The experimental operating condition was optimized and was seen that ozone generation rate of 1.33 mg s
MeSH term(s)	Cyanides ; Electrocoagulation ; Industrial Waste ; Ozone ; Steel ; Waste Disposal, Fluid ; Waste Water ; Water Pollutants, Chemical
Chemical Substances	Cyanides ; Industrial Waste ; Waste Water ; Water Pollutants, Chemical ; Steel (12597-69-2) ; Ozone (66H7ZZK23N)
Language	English
Publishing date	2020-09-18
Publishing country	England
Document type	Journal Article
ZDB-ID	120089-6
ISSN	1879-1298 ; 0045-6535 ; 0366-7111
ISSN (online)	1879-1298
ISSN	0045-6535 ; 0366-7111
DOI	10.1016/j.chemosphere.2020.128370
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