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Article ; Online: A review on development of metal-organic framework-derived bifunctional electrocatalysts for oxygen electrodes in metal-air batteries.

Javed, Najla / Noor, Tayyaba / Iqbal, Naseem / Naqvi, Salman Raza

RSC advances

2023 Volume 13, Issue 2, Page(s) 1137–1161

Abstract: Worldwide demand for oil, coal, and natural gas has increased recently because of odd weather patterns and economies recovering from the pandemic. By using these fuels at an astonishing rate, their reserves are running low with each passing decade. ... ...

Abstract	Worldwide demand for oil, coal, and natural gas has increased recently because of odd weather patterns and economies recovering from the pandemic. By using these fuels at an astonishing rate, their reserves are running low with each passing decade. Increased reliance on these sources is contributing significantly to both global warming and power shortage problems. It is vital to highlight and focus on using renewable energy sources for power production and storage. This review aims to discuss one of the cutting-edge technologies, metal-air batteries, which are currently being researched for energy storage applications. A battery that employs an external cathode of ambient air and an anode constructed of pure metal in which an electrolyte can be aqueous or aprotic electrolyte is termed as a metal-air battery (MAB). Due to their reportedly higher energy density, MABs are frequently hailed as the electrochemical energy storage of the future for applications like grid storage or electric car energy storage. The demand of the upcoming energy storage technologies can be satisfied by these MABs. The usage of metal-organic frameworks (MOFs) in metal-air batteries as a bi-functional electrocatalyst has been widely studied in the last decade. Metal ions or arrays bound to organic ligands to create one, two, or three-dimensional structures make up the family of molecules known as MOFs. They are a subclass of coordination polymers; metal nodes and organic linkers form different classes of these porous materials. Because of their modular design, they offer excellent synthetic tunability, enabling precise chemical and structural control that is highly desirable in electrode materials of MABs.
Language	English
Publishing date	2023-01-16
Publishing country	England
Document type	Journal Article ; Review
ISSN	2046-2069
ISSN (online)	2046-2069
DOI	10.1039/d2ra06741b
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Article ; Online: An integrated approach for the extraction of lipids from marine macroalgae consortium using RSM optimization and thermo-kinetic analysis.

AlMohamadi, Hamad / Alamoudi, Majed / Yameen, Muhammad Zubair / Naqvi, Salman Raza

Chemosphere

2023 Volume 338, Page(s) 139623

Abstract: This work presents an integrated approach for the extraction of lipids from marine macroalgae using RSM optimization and thermo-kinetic analysis. The lipids were extracted from marine macroalgal biomass using a Soxhlet extractor. The Soxhlet extraction ... ...

Abstract	This work presents an integrated approach for the extraction of lipids from marine macroalgae using RSM optimization and thermo-kinetic analysis. The lipids were extracted from marine macroalgal biomass using a Soxhlet extractor. The Soxhlet extraction parameters, including temperature (60-80 °C), solvent-to-algae ratio (3:1-7:1), algal particle size (0.05-0.25 mm), and extraction time (60-180 min), were optimized using RSM to achieve the maximum possible lipid extraction yield from marine macroalgae. The highest lipid extraction yield of 12.76% was obtained using the optimized conditions, which included an extraction temperature of 72 °C, a solvent-to-algae ratio of 5:1, an algal particle size of 0.16 mm, and an extraction time of 134 min. The kinetic analysis revealed an activation energy of 52.79 kJ mol-1 for the Soxhlet extraction process. The thermodynamic analysis of the Soxhlet extraction process demonstrated the following results: ΔH = 49.98 kJ mol-1, ΔS = -128.24 J K-1 mol-1, and ΔG = 93.98 kJ mol-1. The GC-MS analysis confirmed that the extracted algal lipids exhibited a composition of 14.20% palmitic acid, 4.89% stearic acid, and 76.97% oleic acid. The physiochemical analysis ensured that the extracted algal lipids possess excellent qualities, making them desirable for sustainable biofuel production.
MeSH term(s)	Kinetics ; Seaweed ; Temperature ; Thermodynamics ; Solvents ; Lipids/analysis
Chemical Substances	Solvents ; Lipids
Language	English
Publishing date	2023-07-22
Publishing country	England
Document type	Journal Article
ZDB-ID	120089-6
ISSN	1879-1298 ; 0045-6535 ; 0366-7111
ISSN (online)	1879-1298
ISSN	0045-6535 ; 0366-7111
DOI	10.1016/j.chemosphere.2023.139623
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Article ; Online: An integrated approach for the extraction of lipids from marine macroalgae consortium using RSM optimization and thermo-kinetic analysis

AlMohamadi, Hamad / Alamoudi, Majed / Yameen, Muhammad Zubair / Naqvi, Salman Raza

Chemosphere. 2023 Oct., v. 338 p.139623-

2023

Abstract	This work presents an integrated approach for the extraction of lipids from marine macroalgae using RSM optimization and thermo-kinetic analysis. The lipids were extracted from marine macroalgal biomass using a Soxhlet extractor. The Soxhlet extraction parameters, including temperature (60–80 °C), solvent-to-algae ratio (3:1–7:1), algal particle size (0.05–0.25 mm), and extraction time (60–180 min), were optimized using RSM to achieve the maximum possible lipid extraction yield from marine macroalgae. The highest lipid extraction yield of 12.76% was obtained using the optimized conditions, which included an extraction temperature of 72 °C, a solvent-to-algae ratio of 5:1, an algal particle size of 0.16 mm, and an extraction time of 134 min. The kinetic analysis revealed an activation energy of 52.79 kJ mol−1 for the Soxhlet extraction process. The thermodynamic analysis of the Soxhlet extraction process demonstrated the following results: ΔH = 49.98 kJ mol−1, ΔS = −128.24 J K−1 mol−1, and ΔG = 93.98 kJ mol−1. The GC-MS analysis confirmed that the extracted algal lipids exhibited a composition of 14.20% palmitic acid, 4.89% stearic acid, and 76.97% oleic acid. The physiochemical analysis ensured that the extracted algal lipids possess excellent qualities, making them desirable for sustainable biofuel production.
Keywords	activation energy ; biomass ; fuel production ; kinetics ; macroalgae ; oleic acid ; palmitic acid ; particle size ; solid phase extraction ; stearic acid ; temperature ; Marine macroalgae ; Algal lipids ; Soxhlet extraction ; RSM optimization ; Thermodynamics
Language	English
Dates of publication	2023-10
Publishing place	Elsevier Ltd
Document type	Article ; Online
ZDB-ID	120089-6
ISSN	1879-1298 ; 0045-6535 ; 0366-7111
ISSN (online)	1879-1298
ISSN	0045-6535 ; 0366-7111
DOI	10.1016/j.chemosphere.2023.139623
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Article ; Online: Life cycle assessment of a biomass based chemical looping combustion.

Mercado, John Patrick / Ubando, Aristotle T / Gonzaga, Jeremias A / Naqvi, Salman Raza

Environmental research

2022 Volume 217, Page(s) 114876

Abstract: Chemical looping combustion (CLC) is a promising technology that generates energy while inherently separating carbon dioxide from air using oxygen carriers. This allows for an efficient and cost-effective means of carbon capture and storage. Current CLC ... ...

Abstract	Chemical looping combustion (CLC) is a promising technology that generates energy while inherently separating carbon dioxide from air using oxygen carriers. This allows for an efficient and cost-effective means of carbon capture and storage. Current CLC systems use coal with metal oxides for combustion in the fuel reactor, thus, resulting in some environmental impacts. Recent life cycle assessment (LCA) of CLC studies have indicated the environmental impacts of conventional coal-based CLC, especially on the global warming potential. To mitigate these environmental impacts, this study proposes the use of a biomass-based CLC and evaluates its impacts using LCA. A case study in the Philippines is adopted where rice husks are used as biomass feedstock. A kilowatt-hour of electricity generated from the CLC plant is utilized as the functional unit. A relative comparison of environmental impacts was considered between the coal-based power plant, the coal-based CLC plant, and the biomass-based CLC plant. The single score results have shown that the biomass-based CLC has the least environmental impacts relative to the coal-based power plant and the coal-based CLC plant. However, it is noted that water consumption is the main drawback of utilizing rice husks as CLC biomass feedstock. The majority of the environmental impacts of the coal-based CLC and the coal-based power plant were derived from upstream processes such as coal mining and processing. With the use of rice husks as CLC biomass feedstock, net negative emissions were achieved.
MeSH term(s)	Animals ; Biomass ; Coal ; Oxides ; Carbon Dioxide ; Life Cycle Stages
Chemical Substances	Coal ; Oxides ; Carbon Dioxide (142M471B3J)
Language	English
Publishing date	2022-11-23
Publishing country	Netherlands
Document type	Journal Article ; Research Support, Non-U.S. Gov't
ZDB-ID	205699-9
ISSN	1096-0953 ; 0013-9351
ISSN (online)	1096-0953
ISSN	0013-9351
DOI	10.1016/j.envres.2022.114876
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Article ; Online: Algal-derived biochar as an efficient adsorbent for removal of Cr (VI) in textile industry wastewater: Non-linear isotherm, kinetics and ANN studies.

Khan, Abdul Ahad / Naqvi, Salman Raza / Ali, Imtiaz / Arshad, Muazzam / AlMohamadi, Hamad / Sikandar, Umair

Chemosphere

2023 Volume 316, Page(s) 137826

Abstract: Textile industries release effluent that contains the vast majority of heavy metals in which Cr (VI) is a toxic carcinogenic element that causes an environmental problem. The aim of the work is to synthesize algae-derived biochar derived from algae using ...

Abstract	Textile industries release effluent that contains the vast majority of heavy metals in which Cr (VI) is a toxic carcinogenic element that causes an environmental problem. The aim of the work is to synthesize algae-derived biochar derived from algae using slow pyrolysis at an operating temperature of 500 °C, a heating rate of 10 °C/min and a residence time of 60 min and to use it as an adsorbent to remove Cr (VI). The batch experiment was carried out using different concentrations of Cr (VI) (1, 10, 25, 50, 100, 125, 150 and 200 ppm) at different intervals of time (2.5, 5, 10, 15, 30, 60, 120 and 240 min). The maximum removal percentage of Cr (VI) is 97.88% for the metal concentration of 1 ppm exhibiting non-linear adsorption isotherm (Langmuir, Freundlich, Dubinin-Radushkevich, and Temkin models) and kinetic models (pseudo-first order, pseudo-second order, nth order, and intra-particle diffusion) were analyzed using a solver add-in of Microsoft Excel. According to the results, the Langmuir isotherm model (R
MeSH term(s)	Chromium/analysis ; Wastewater ; Textile Industry ; Water Pollutants, Chemical ; Hydrogen-Ion Concentration ; Charcoal ; Kinetics ; Adsorption
Chemical Substances	Chromium (0R0008Q3JB) ; biochar ; Wastewater ; Water Pollutants, Chemical ; Charcoal (16291-96-6)
Language	English
Publishing date	2023-01-11
Publishing country	England
Document type	Journal Article
ZDB-ID	120089-6
ISSN	1879-1298 ; 0045-6535 ; 0366-7111
ISSN (online)	1879-1298
ISSN	0045-6535 ; 0366-7111
DOI	10.1016/j.chemosphere.2023.137826
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Article ; Online: Development of high-capacity surface-engineered MXene composite for heavy metal Cr (VI) removal from industrial wastewater.

Asif, Umair Ali / Mahmood, Khalid / Naqvi, Salman Raza / Mehran, Muhammad Taqi / Noor, Tayyaba

Chemosphere

2023 Volume 326, Page(s) 138448

Abstract: The substantial quantity of Cr(VI) contaminants in the aqueous atmosphere is a major environmental fear that cannot be overlooked. For the first time, MXene and chitosan-coated polyurethane foam have been employed for wastewater treatment, including ... ...

Abstract	The substantial quantity of Cr(VI) contaminants in the aqueous atmosphere is a major environmental fear that cannot be overlooked. For the first time, MXene and chitosan-coated polyurethane foam have been employed for wastewater treatment, including heavy metal ions (Cr (VI)) through a fixed-bed column study. It is also the most inexpensive, lightweight, and globally friendly material tested. The Mxene and chitosan-coated polyurethane foam hybrid materials were thoroughly investigated using FTIR (Fourier transform infrared), SEM (scanning electron microscope), XPS (X-ray photoelectron spectroscopy) and XRD (X-ray diffraction). The presence of the rough surface and the pore creation in the Mxene- MX
MeSH term(s)	Wastewater ; Chitosan/chemistry ; Water Pollutants, Chemical/analysis ; Chromium/chemistry ; Water/chemistry ; Ions ; Adsorption ; Hydrogen-Ion Concentration ; Kinetics ; Spectroscopy, Fourier Transform Infrared
Chemical Substances	chromium hexavalent ion (18540-29-9) ; polyurethane foam (9009-54-5) ; Wastewater ; Chitosan (9012-76-4) ; MXene ; Water Pollutants, Chemical ; Chromium (0R0008Q3JB) ; Water (059QF0KO0R) ; Ions
Language	English
Publishing date	2023-03-20
Publishing country	England
Document type	Journal Article
ZDB-ID	120089-6
ISSN	1879-1298 ; 0045-6535 ; 0366-7111
ISSN (online)	1879-1298
ISSN	0045-6535 ; 0366-7111
DOI	10.1016/j.chemosphere.2023.138448
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Article ; Online: Assessment of thermokinetic behaviour of tannery sludge in slow pyrolysis process through artificial neural network

Khan, Arslan / Ali, Imtiaz / Naqvi, Salman Raza / AlMohamadi, Hamad / Shahbaz, Muhammad / Ali, Arshid Mahmood / Shahzad, Khurram

Chemosphere. 2023 Oct., v. 337 p.139226-

2023

Abstract: In the leather industry, tannery sludge is produced in large volume. This study investigated the thermal degradation behavior of tannery sludge using thermogravimetric analysis (TGA). The experiments were carried out in an inert atmosphere using nitrogen ...

Abstract	In the leather industry, tannery sludge is produced in large volume. This study investigated the thermal degradation behavior of tannery sludge using thermogravimetric analysis (TGA). The experiments were carried out in an inert atmosphere using nitrogen gas at varied heating rates of 5, 10, 20, and 40 °C/min in the temperature range of 30–900 °C. For the kinetic parameters calculation, three different models, Friedman, Kissinger-Akahira-Sunose (KAS) and the Ozawa-Flynn-Wall (OFW), were employed. The average activation energy (Eₐ) obtained from Friedman, KAS, and the OFW methods were 130.9 kJ mol⁻¹, 143.14 kJ mol⁻¹, and 147.19 kJ mol⁻¹ respectively. Along with that, experiment of pyrolysis was accomplished in fixed bed reactor (FBR) at temperature of 400 °C. Biochar produced from FBR had a yield of about 71%. The analysis of gas chromatography-mass spectroscopy shows the different chemical compounds present in the bio-oil containing hydrocarbons (alkanes and alkenes), oxygen containing compounds (alcohols, aldehyde, ketones, esters carboxylic acids and the esters) and the nitrogen containing compounds. The kinetic assessment was complemented by distributed activation energy model (DAEM). In the pyrolysis of tannery sludge six pseudo-components were found to be involved. Furthermore, artificial neural network (ANN) was used to predict the activation energy from conversion, temperature, and the heating rate data. MLP-3-11-1 (Multilayer Perceptrons) described well the conversion behavior of tannery sludge pyrolysis.
Keywords	activation energy ; aldehydes ; alkenes ; biochar ; biofuels ; gas chromatography ; leather industry ; neural networks ; nitrogen ; oxygen ; pyrolysis ; spectroscopy ; tannery waste ; temperature ; thermogravimetry ; Tannery sludge pyrolysis ; Isoconversional ; Thermodynamics ; DAEM ; ANN
Language	English
Dates of publication	2023-10
Publishing place	Elsevier Ltd
Document type	Article ; Online
ZDB-ID	120089-6
ISSN	1879-1298 ; 0045-6535 ; 0366-7111
ISSN (online)	1879-1298
ISSN	0045-6535 ; 0366-7111
DOI	10.1016/j.chemosphere.2023.139226
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Article: Monitoring lipids profile, CO2 fixation, and water recyclability for the economic viability of microalgae Chlorella vulgaris cultivation at different initial nitrogen

Farooq, Wasif / Naqvi, Salman Raza / Sajid, Muhammad / Shrivastav, Anupama / Kumar, Kanhaiya

Journal of biotechnology. 2022 Feb. 10, v. 345

2022

Abstract: The economic viability of microalgae as a bioenergy source depends on many factors. High CO₂ fixing rate, improved lipids yield, and minimum water footprint are few key parameters. This study investigates the effect of four initial nitrogen ... ...

Abstract	The economic viability of microalgae as a bioenergy source depends on many factors. High CO₂ fixing rate, improved lipids yield, and minimum water footprint are few key parameters. This study investigates the effect of four initial nitrogen concentrations (1-, 2-, 6- and 10-mM as nitrate) on lipids yield, their classification and composition, CO₂ fixation rate, and water quality for further reuse after first cultivation. The initial 6 mM nitrate was found optimum for the growth and overall lipid productivity of Chlorella vulgaris. The maximum quantum efficiency (as Fv/Fm ratio) for algae decreases along with the cell growth profile and depletion of the initial nitrate concentration. CO₂ fixation rate increased initially and peaked during exponential growth and then declined for the rest of the cultivation period. A higher CO₂ fixation rate was recorded at 6 mM, and an overall fixation rate of CO₂ was high at 6 mM. A higher total organic carbon (TOC) is produced in recycled water at a low nitrogen concentration of 1 and 2 mM. TOC changes during the cultivation period and with each reuse of water. Water was recycled twice successfully, while growth was inhibited during the 3rd cycle. Based on all these investigations, 6 mM of initial nitrogen was found optimal at given growth conditions.
Keywords	Chlorella vulgaris ; bioenergy ; biotechnology ; carbon dioxide ; carbon dioxide fixation ; cell growth ; economic sustainability ; lipids ; microalgae ; nitrates ; nitrogen ; nitrogen content ; recycled water ; total organic carbon ; water footprint ; water quality ; water reuse
Language	English
Dates of publication	2022-0210
Size	p. 30-39.
Publishing place	Elsevier B.V.
Document type	Article
ZDB-ID	843647-2
ISSN	1873-4863 ; 0168-1656 ; 1389-0352
ISSN (online)	1873-4863
ISSN	0168-1656 ; 1389-0352
DOI	10.1016/j.jbiotec.2021.12.014
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Article: Comparative hydrodynamics study of fluidized bed gasifier incorporating static and rotating air distributor plates: A CFD approach

Raza, Naveed / Ahsan, Muhammad / Mehran, Muhammad Taqi / Naqvi, Salman Raza / Ahmad, Iftikhar

Powder technology. 2022 June, v. 405

2022

Abstract: This paper studies hydrodynamics of bubbling fluidized bed gasifier using static and rotating perforated air distributor plates. Pressure drop across the bed is calculated numerically using a static distributor plate to validate the model results with ... ...

Abstract	This paper studies hydrodynamics of bubbling fluidized bed gasifier using static and rotating perforated air distributor plates. Pressure drop across the bed is calculated numerically using a static distributor plate to validate the model results with available experimental data. CFD results are good enough within the acceptable range of 10% difference. Dynamic mesh methodology coupled with the siding mesh technique of ANSYS FLUENT is incorporated to rotate distributor plates for specified rotational velocity using a user-defined function (UDF) hooked to the solver. Hydrodynamics study of fluidized bed with varying operational parameters using rotating plate distributor is carried out extensively. It is revealed that the impact of tangential and radial velocities on the fluidized bed due to rotation of plate is highest for lower superficial velocities, shallow initial depth, and the maximum rotational velocity of the distributor plate. The tangential and radial velocities variations with column height up to 3Uₘf showed a similar trend that changed significantly for higher superficial velocities (4Uₘf, 5Uₘf), resulting in more chaotic solids. The comparative evaluation of static and rotating distributor plates results shows an appreciable difference. The pressure drop across the bed is increased about 6–7% and minimum fluidization velocity is decreased upto 10% when compared to static plate distributor. Moreover, bed height rise is on a higher side for static plate distributors due to the dominant axial component of air velocity compared to the rotating plate distributor. It is also revealed that the pressure fluctuations within the fluidized bed are significantly reduced (88%) when using a rotating distributor plate compared with static plate distributors.
Keywords	air ; fluidized beds ; hydrodynamics ; model validation ; technology
Language	English
Dates of publication	2022-06
Publishing place	Elsevier B.V.
Document type	Article
ISSN	0032-5910
DOI	10.1016/j.powtec.2022.117500
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Article ; Online: Monitoring lipids profile, CO

Farooq, Wasif / Naqvi, Salman Raza / Sajid, Muhammad / Shrivastav, Anupama / Kumar, Kanhaiya

Journal of biotechnology

2022 Volume 345, Page(s) 30–39

Abstract: The economic viability of microalgae as a bioenergy source depends on many factors. High ... ...

Abstract	The economic viability of microalgae as a bioenergy source depends on many factors. High CO
MeSH term(s)	Biofuels ; Biomass ; Carbon Dioxide ; Chlorella vulgaris ; Lipids ; Microalgae ; Nitrogen/analysis ; Waste Water
Chemical Substances	Biofuels ; Lipids ; Waste Water ; Carbon Dioxide (142M471B3J) ; Nitrogen (N762921K75)
Language	English
Publishing date	2022-01-04
Publishing country	Netherlands
Document type	Journal Article ; Review
ZDB-ID	843647-2
ISSN	1873-4863 ; 0168-1656 ; 1389-0352
ISSN (online)	1873-4863
ISSN	0168-1656 ; 1389-0352
DOI	10.1016/j.jbiotec.2021.12.014
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