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  1. AU="Pinter, Emily N"
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  1. Article ; Online: Fluorosulfonamide-Directed Heteroarylation of Aliphatic C(sp

    Pinter, Emily N / Sheldon, Zachary S / Modak, Atanu / Cook, Silas P

    The Journal of organic chemistry

    2023  Volume 88, Issue 7, Page(s) 4757–4760

    Abstract: Herein, we describe a formal dehydrogenative cross coupling of heterocycles with unactivated aliphatic amines. The resulting transformation enables the direct alkylation of common heterocycles by merging N-F-directed 1,5-HAT with Minisci chemistry, ... ...

    Abstract Herein, we describe a formal dehydrogenative cross coupling of heterocycles with unactivated aliphatic amines. The resulting transformation enables the direct alkylation of common heterocycles by merging N-F-directed 1,5-HAT with Minisci chemistry, leading to predictable site selectivity. The reaction provides a direct route for the transformation of simple alkyl amines to value-added products under mild reaction conditions, making this an attractive option for C(sp
    Language English
    Publishing date 2023-03-13
    Publishing country United States
    Document type Journal Article
    ZDB-ID 123490-0
    ISSN 1520-6904 ; 0022-3263
    ISSN (online) 1520-6904
    ISSN 0022-3263
    DOI 10.1021/acs.joc.2c02461
    Database MEDical Literature Analysis and Retrieval System OnLINE

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    In stock of ZB MED Cologne/Königswinter

    Zs.A 4473: Show issues Location:
    Je nach Verfügbarkeit (siehe Angabe bei Bestand)
    bis Jg. 1994: Bestellungen von Artikeln über das Online-Bestellformular
    Jg. 1995 - 2021: Lesesall (2.OG)
    ab Jg. 2022: Lesesaal (EG)

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  2. Article ; Online: Copper-Catalyzed, N-Directed Csp

    Modak, Atanu / Pinter, Emily N / Cook, Silas P

    Journal of the American Chemical Society

    2019  Volume 141, Issue 46, Page(s) 18405–18410

    Abstract: A direct and versatile copper-catalyzed trifluoromethylthiolation and trifluoromethylselenation of primary, secondary, and tertiary aliphatic C-H bonds was developed. The reaction provides direct access to molecules containing these emerging moieties in ... ...

    Abstract A direct and versatile copper-catalyzed trifluoromethylthiolation and trifluoromethylselenation of primary, secondary, and tertiary aliphatic C-H bonds was developed. The reaction provides direct access to molecules containing these emerging moieties in the presence of a wide range of common functional groups and in complex molecular environments.
    MeSH term(s) Catalysis ; Copper/chemistry ; Fluorine/chemistry ; Halogenation ; Methylation ; Organoselenium Compounds/chemical synthesis ; Organoselenium Compounds/chemistry ; Sulfhydryl Compounds/chemical synthesis ; Sulfhydryl Compounds/chemistry
    Chemical Substances Organoselenium Compounds ; Sulfhydryl Compounds ; Fluorine (284SYP0193) ; Copper (789U1901C5)
    Language English
    Publishing date 2019-11-07
    Publishing country United States
    Document type Journal Article ; Research Support, N.I.H., Extramural ; Research Support, Non-U.S. Gov't ; Research Support, U.S. Gov't, Non-P.H.S.
    ZDB-ID 3155-0
    ISSN 1520-5126 ; 0002-7863
    ISSN (online) 1520-5126
    ISSN 0002-7863
    DOI 10.1021/jacs.9b10316
    Database MEDical Literature Analysis and Retrieval System OnLINE

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    In stock of ZB MED Bonn / Germany

    Z 4' 55/32: Show issues
    Z 7.3: Show issues

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  3. Article: N-Directed fluorination of unactivated Csp

    Pinter, Emily N / Bingham, Jenna E / AbuSalim, Deyaa I / Cook, Silas P

    Chemical science

    2019  Volume 11, Issue 4, Page(s) 1102–1106

    Abstract: Site-selective fluorination of aliphatic C-H bonds remains synthetically challenging. While directed C-H fluorination represents the most promising approach, the limited work conducted to date has enabled just a few functional groups as the arbiters of ... ...

    Abstract Site-selective fluorination of aliphatic C-H bonds remains synthetically challenging. While directed C-H fluorination represents the most promising approach, the limited work conducted to date has enabled just a few functional groups as the arbiters of direction. Leveraging insights gained from both computations and experimentation, we enabled the use of the ubiquitous amine functional group as a handle for the directed C-H fluorination of Csp
    Language English
    Publishing date 2019-12-16
    Publishing country England
    Document type Journal Article
    ZDB-ID 2559110-1
    ISSN 2041-6539 ; 2041-6520
    ISSN (online) 2041-6539
    ISSN 2041-6520
    DOI 10.1039/c9sc04055b
    Database MEDical Literature Analysis and Retrieval System OnLINE

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