Article: Pretreatment methods for determination of Mei-ting residue in fish muscle by high performance liquid chromatography
Journal of Huazhong Agricultural University
Dec.2013 , Issue (6)
Abstract: 对高效液相色谱法测定草鱼和鲫肌肉组织中＂美婷＂原料药残留的前处理方法进行探讨。结果表明：以甲醇作抽提剂、二氯甲烷作净化剂，振荡离心，正己烷去脂，30℃旋转浓缩蒸发的前处理方法，快速、准确、经济、实用性强。该方法＂美婷＂原料药的最低检测限可达1.0μg/kg；在加标水平为1.0-100μg/kg时，回收率为67.72%-95.52%；相对标准偏差为7.76%-37.81%。该前处理方法适合检测＂美婷＂原料药在鱼体内的残留。 ...
| Abstract | 对高效液相色谱法测定草鱼和鲫肌肉组织中＂美婷＂原料药残留的前处理方法进行探讨。结果表明：以甲醇作抽提剂、二氯甲烷作净化剂，振荡离心，正己烷去脂，30℃旋转浓缩蒸发的前处理方法，快速、准确、经济、实用性强。该方法＂美婷＂原料药的最低检测限可达1.0μg/kg；在加标水平为1.0-100μg/kg时，回收率为67.72%-95.52%；相对标准偏差为7.76%-37.81%。该前处理方法适合检测＂美婷＂原料药在鱼体内的残留。 |
|---|---|
| Keywords | FISHES ; MUSCLES ; HPLC ; POISSON (ANIMAL) ; MUSCLE ; HPLC ; PECES ; MUSCULOS ; HPLC ; http://www.fao.org/aos/agrovoc#c_2943 ; http://www.fao.org/aos/agrovoc#c_5003 ; http://www.fao.org/aos/agrovoc#c_24469 |
| Language | zho |
| Document type | Article |
| ISSN | 1000-2421 |
| Database | AGRIS - International Information System for the Agricultural Sciences and Technology |
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