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Article ; Online: Development of a UPLC-MS/MS-based method for simultaneous determination of advanced glycation end products and heterocyclic amines in stewed meat products.

Wang, Tan / Dong, Maofeng / Shen, Qinyi / Wen, Guangyue / Wang, Mingfu / Zhao, Yueliang

2024 Volume 451, Page(s) 139470

Abstract: A novel analytical strategy was proposed to simultaneously quantify two advanced glycation end products (AGEs) including ... ...

Abstract	A novel analytical strategy was proposed to simultaneously quantify two advanced glycation end products (AGEs) including N
Language	English
Publishing date	2024-04-23
Publishing country	England
Document type	Journal Article
ZDB-ID	243123-3
ISSN	1873-7072 ; 0308-8146
ISSN (online)	1873-7072
ISSN	0308-8146
DOI	10.1016/j.foodchem.2024.139470
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Article: Long-Distance Wind Dispersal Drives Population Range Expansion of

Zhang, Zheng / Wen, Guangyue / Bu, Dexiao / Sun, Guojun / Qiang, Sheng

Plants (Basel, Switzerland)

2022 Volume 11, Issue 20

Abstract: Canada goldenrod ( ...

Abstract	Canada goldenrod (
Language	English
Publishing date	2022-10-16
Publishing country	Switzerland
Document type	Journal Article
ZDB-ID	2704341-1
ISSN	2223-7747
ISSN	2223-7747
DOI	10.3390/plants11202734
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Article ; Online: Residue behaviors, degradation, processing factors, and risk assessment of pesticides in citrus from field to product processing

Tang, Hongxia / Sun, Qiang / Huang, Jiaqing / Wen, Guangyue / Han, Lijun / Wang, Lei / Zhang, Ying / Dong, Maofeng / Wang, Weimin

Science of the Total Environment. 2023 Nov., v. 897 p.165321-

2023

Abstract: Pesticide residues in citrus may cause health risks in related juice products, and bring much uncertainty during the processing procedures. In this study, based on the dispersive solid-phase extraction (d-SPE) and UPLC–MS/MS, the residual levels of ten ... ...

Abstract	Pesticide residues in citrus may cause health risks in related juice products, and bring much uncertainty during the processing procedures. In this study, based on the dispersive solid-phase extraction (d-SPE) and UPLC–MS/MS, the residual levels of ten analytes in citrus and its processed products were monitored. The results showed that dissipation of the pesticides followed the first-order kinetics and the half-lives in citrus varied greatly, ranging from 6.36 to 63.0 days. The terminal residues of the five pesticides at harvest time were <0.01–0.302 and <0.01–0.124 mg/kg in raw citrus and citrus flesh, respectively, all of which were lower than the corresponding maximum residue limits (MRLs) of 0.5–1 mg/kg. In the processing experiments, the residues of ten analytes in sterilized juice, concentrated juice, and citrus essential oil were in the range of <0.01 to 0.442 mg/kg, <0.01 to 1.16 mg/kg, and <0.01 to 44.0 mg/kg, respectively, and the corresponding processing factors (PFs) were 0.127–1.00, 0.023–3.06, and 0.006–39.2. Particularly, in citrus essential oil, the PFs of etoxazole, fluazinam, lufenuron and spirotetramat-keto-hydroxy were 1.68–39.2, exhibiting obvious enrichment effects. By integrating the residue data of the field trials and the PFs, the acute and chronic dietary risks of the target pesticides in citrus juice were 0.031–1.83 % and 0.002–2.51 %, respectively, which were far lower than 100 %, demonstrating no unacceptable risk to human health. This work provides basic data for the establishment of the MRLs and dietary exposure risk assessment for processed citrus products.
Keywords	Citrus ; chemical species ; citrus juices ; dietary exposure ; environment ; essential oils ; etoxazole ; half life ; harvest date ; human health ; lufenuron ; risk ; risk assessment ; solid phase extraction ; uncertainty ; Processing factors ; Dissipation ; Residue levels
Language	English
Dates of publication	2023-11
Publishing place	Elsevier B.V.
Document type	Article ; Online
ZDB-ID	121506-1
ISSN	1879-1026 ; 0048-9697
ISSN (online)	1879-1026
ISSN	0048-9697
DOI	10.1016/j.scitotenv.2023.165321
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Article: [Determination of disulfoton and its metabolites in agricultural products by dispersive soild phase extraction-ultra high performance liquid chromatography-tandem mass spectrometry].

Sun, Qiang / Li, Yubo / Wen, Guangyue / Wang, Weimin / Dong, Maofeng / Tang, Hongxia

Se pu = Chinese journal of chromatography

2022 Volume 40, Issue 2, Page(s) 130–138

Abstract: Disulfoton, an organophosphorus pesticide, is used to control cotton, beet, potato, and other seedling period aphids, leaf moths, underground pests, etc., with internal absorption, killing, gastric poisoning, and fumigation. Disulfoton is a highly toxic ... ...

Abstract	Disulfoton, an organophosphorus pesticide, is used to control cotton, beet, potato, and other seedling period aphids, leaf moths, underground pests, etc., with internal absorption, killing, gastric poisoning, and fumigation. Disulfoton is a highly toxic organophosphate pesticide, which can inhibit cholinesterase activity, resulting in neurophysiological disorders by inhalation, feeding, and transdermal absorption. Disulfoton is difficult to degrade in the environment, which leads to enrichment in organisms and interference with endocrine. This compound is harmful to the ecological environment and human health. To ensure the quality and safety of food, it is important to develop a detection method for disulfoton and its metabolites in agricultural products. A reliable method based on dispersive solid phase extraction (d-SPE) with ultra high performance liquid chromatography-tandem mass spectrometry (UHPLC-MS/MS) was developed for the determination of disulfoton and its metabolites (disulfoton sulfone, disulfoton sulfoxide, demeton-
MeSH term(s)	Chromatography, High Pressure Liquid ; Disulfoton ; Humans ; Nanotubes, Carbon ; Organophosphorus Compounds ; Pesticides ; Solid Phase Extraction ; Tandem Mass Spectrometry
Chemical Substances	Nanotubes, Carbon ; Organophosphorus Compounds ; Pesticides ; Disulfoton (3CY5EKL6MT)
Language	Chinese
Publishing date	2022-01-25
Publishing country	China
Document type	Journal Article
ISSN	1000-8713
ISSN	1000-8713
DOI	10.3724/SP.J.1123.2021.04028
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Article ; Online: Residue behaviors, degradation, processing factors, and risk assessment of pesticides in citrus from field to product processing.

Tang, Hongxia / Sun, Qiang / Huang, Jiaqing / Wen, Guangyue / Han, Lijun / Wang, Lei / Zhang, Ying / Dong, Maofeng / Wang, Weimin

The Science of the total environment

2023 Volume 897, Page(s) 165321

Abstract	Pesticide residues in citrus may cause health risks in related juice products, and bring much uncertainty during the processing procedures. In this study, based on the dispersive solid-phase extraction (d-SPE) and UPLC-MS/MS, the residual levels of ten analytes in citrus and its processed products were monitored. The results showed that dissipation of the pesticides followed the first-order kinetics and the half-lives in citrus varied greatly, ranging from 6.36 to 63.0 days. The terminal residues of the five pesticides at harvest time were <0.01-0.302 and <0.01-0.124 mg/kg in raw citrus and citrus flesh, respectively, all of which were lower than the corresponding maximum residue limits (MRLs) of 0.5-1 mg/kg. In the processing experiments, the residues of ten analytes in sterilized juice, concentrated juice, and citrus essential oil were in the range of <0.01 to 0.442 mg/kg, <0.01 to 1.16 mg/kg, and <0.01 to 44.0 mg/kg, respectively, and the corresponding processing factors (PFs) were 0.127-1.00, 0.023-3.06, and 0.006-39.2. Particularly, in citrus essential oil, the PFs of etoxazole, fluazinam, lufenuron and spirotetramat-keto-hydroxy were 1.68-39.2, exhibiting obvious enrichment effects. By integrating the residue data of the field trials and the PFs, the acute and chronic dietary risks of the target pesticides in citrus juice were 0.031-1.83 % and 0.002-2.51 %, respectively, which were far lower than 100 %, demonstrating no unacceptable risk to human health. This work provides basic data for the establishment of the MRLs and dietary exposure risk assessment for processed citrus products.
MeSH term(s)	Humans ; Pesticides/analysis ; Tandem Mass Spectrometry/methods ; Chromatography, Liquid ; Citrus ; Pesticide Residues/analysis ; Fruit/chemistry ; Risk Assessment
Chemical Substances	Pesticides ; Pesticide Residues
Language	English
Publishing date	2023-07-06
Publishing country	Netherlands
Document type	Journal Article
ZDB-ID	121506-1
ISSN	1879-1026 ; 0048-9697
ISSN (online)	1879-1026
ISSN	0048-9697
DOI	10.1016/j.scitotenv.2023.165321
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Article ; Online: Residue behavior and dietary risk assessment of six pesticides in pak choi using QuEChERS method coupled with UPLC-MS/MS.

Tang, Hongxia / Ma, Lin / Huang, Jiaqing / Li, Yubo / Liu, Zehui / Meng, Dianying / Wen, Guangyue / Dong, Maofeng / Wang, Weimin / Zhao, Li

Ecotoxicology and environmental safety

2021 Volume 213, Page(s) 112022

Abstract: A reliable and simple modified QuEChERS method with UPLC-MS/MS was developed for the simultaneous determination of six pesticides (dimethomorph, imidaclothiz, lufenuron, methoxyfenozide, pyridaben, spinetoram) and their metabolites in pak choi. Method ... ...

Abstract	A reliable and simple modified QuEChERS method with UPLC-MS/MS was developed for the simultaneous determination of six pesticides (dimethomorph, imidaclothiz, lufenuron, methoxyfenozide, pyridaben, spinetoram) and their metabolites in pak choi. Method validation indicated good linearity (R
MeSH term(s)	Brassica/chemistry ; China ; Chromatography, High Pressure Liquid ; Chromatography, Liquid/methods ; Dietary Exposure/statistics & numerical data ; Food Safety ; Hydrazines ; Juvenile Hormones ; Macrolides ; Pesticide Residues/analysis ; Pesticides/analysis ; Pesticides/toxicity ; Risk Assessment ; Tandem Mass Spectrometry/methods
Chemical Substances	Hydrazines ; Juvenile Hormones ; Macrolides ; Pesticide Residues ; Pesticides ; methoxyfenozide (62A22651ZX) ; spinetoram (YGZ1037ELN)
Language	English
Publishing date	2021-02-18
Publishing country	Netherlands
Document type	Journal Article
ZDB-ID	436536-7
ISSN	1090-2414 ; 0147-6513
ISSN (online)	1090-2414
ISSN	0147-6513
DOI	10.1016/j.ecoenv.2021.112022
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Jg. 1995 - 2021: Lesesall (1.OG)
ab Jg. 2022: Lesesaal (EG)

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Article ; Online: Determination of 1-methylcyclopropene residues in vegetables and fruits based on iodine derivatives.

Dong, Maofeng / Wen, Guangyue / Li, Junshun / Wang, Tan / Huang, Jiaqing / Li, Yubo / Tang, Hongxia / Sun, Qiang / Wang, Weimin

Food chemistry

2021 Volume 358, Page(s) 129854

Abstract: An innovative method was established for the determination of 1-methylcyclopropene (1-MCP) in vegetables and fruits. Due to its small molecular weight and low boiling point, it was difficult to obtain quantitative analysis for 1-MCP, especially at the ... ...

Abstract	An innovative method was established for the determination of 1-methylcyclopropene (1-MCP) in vegetables and fruits. Due to its small molecular weight and low boiling point, it was difficult to obtain quantitative analysis for 1-MCP, especially at the residual level. In this work, based on its iodine derivatives, 1-MCP was derived to 1,2-diiodo-1-methylcyclopropane, which was much easier for trace and accurate chromatographic analysis. During the method validation, the method validation results were satisfactory in terms of linearity (4 ~ 400 µg/L, and R
MeSH term(s)	Cyclopropanes/analysis ; Cyclopropanes/chemistry ; Food Analysis/methods ; Food Contamination/analysis ; Fruit/chemistry ; Gas Chromatography-Mass Spectrometry/methods ; Iodine/analysis ; Iodine/chemistry ; Limit of Detection ; Tandem Mass Spectrometry/methods ; Vegetables/chemistry
Chemical Substances	Cyclopropanes ; Iodine (9679TC07X4) ; 1-methylcyclopropene (J6UJO23JGU)
Language	English
Publishing date	2021-04-20
Publishing country	England
Document type	Journal Article
ZDB-ID	243123-3
ISSN	1873-7072 ; 0308-8146
ISSN (online)	1873-7072
ISSN	0308-8146
DOI	10.1016/j.foodchem.2021.129854
Database	MEDical Literature Analysis and Retrieval System OnLINE

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Article: Dissipation and safety evaluation of novaluron, pyriproxyfen, thiacloprid and tolfenpyrad residues in the citrus-field ecosystem

Dong, Maofeng / Wen, Guangyue / Tang, Hongxia / Wang, Tan / Zhao, Zhihui / Song, Weiguo / Wang, Weimin / Zhao, Li

Food chemistry. 2018 Dec. 15, v. 269

2018

Abstract: The dissipations and residues of four pesticides in citrus, under field conditions, were measured using solid-phase extraction and LC-MS/MS. In the method validation, satisfactory results were obtained with fortified recoveries ranging from 80.6 to 113% ... ...

Abstract	The dissipations and residues of four pesticides in citrus, under field conditions, were measured using solid-phase extraction and LC-MS/MS. In the method validation, satisfactory results were obtained with fortified recoveries ranging from 80.6 to 113% and relative standard deviations ≤9.0%. In the dissipation test, the half-lives for the pesticides in citrus, according to first-order kinetics, ranged from 13.3 to 28.9 days. Based on the terminal residue test, two evaluation models (hazard quotient, HQ; risk quotient, RQ) were applied on citrus fruits for dietary exposure risk assessment. The results showed that HQs ranged from 0.0031 to 0.78%, and RQs from 7.3 to 57%, which are both acceptable for human consumption. Therefore, 14-day was proposed as a pre-harvest interval for the target compounds in citrus fruits. This work also contributes to residue data and, therefore, scientifically validated maximum residue limits in citrus, which are lacking in China currently.
Keywords	Citrus ; citrus fruits ; dietary exposure ; ecosystems ; half life ; humans ; maximum residue limits ; models ; novaluron ; pyriproxyfen ; risk ; risk assessment ; solid phase extraction ; statistical analysis ; thiacloprid ; China
Language	English
Dates of publication	2018-1215
Size	p. 136-141.
Publishing place	Elsevier Ltd
Document type	Article
ZDB-ID	243123-3
ISSN	1873-7072 ; 0308-8146
ISSN (online)	1873-7072
ISSN	0308-8146
DOI	10.1016/j.foodchem.2018.07.005
Database	NAL-Catalogue (AGRICOLA)

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Article ; Online: Dissipation and safety evaluation of novaluron, pyriproxyfen, thiacloprid and tolfenpyrad residues in the citrus-field ecosystem.

Dong, Maofeng / Wen, Guangyue / Tang, Hongxia / Wang, Tan / Zhao, Zhihui / Song, Weiguo / Wang, Weimin / Zhao, Li

Food chemistry

2018 Volume 269, Page(s) 136–141

Abstract	The dissipations and residues of four pesticides in citrus, under field conditions, were measured using solid-phase extraction and LC-MS/MS. In the method validation, satisfactory results were obtained with fortified recoveries ranging from 80.6 to 113% and relative standard deviations ≤9.0%. In the dissipation test, the half-lives for the pesticides in citrus, according to first-order kinetics, ranged from 13.3 to 28.9 days. Based on the terminal residue test, two evaluation models (hazard quotient, HQ; risk quotient, RQ) were applied on citrus fruits for dietary exposure risk assessment. The results showed that HQs ranged from 0.0031 to 0.78%, and RQs from 7.3 to 57%, which are both acceptable for human consumption. Therefore, 14-day was proposed as a pre-harvest interval for the target compounds in citrus fruits. This work also contributes to residue data and, therefore, scientifically validated maximum residue limits in citrus, which are lacking in China currently.
MeSH term(s)	China ; Citrus/chemistry ; Ecosystem ; Neonicotinoids/analysis ; Pesticide Residues/analysis ; Phenylurea Compounds/analysis ; Pyrazoles/analysis ; Pyridines/analysis ; Tandem Mass Spectrometry/methods ; Thiazines/analysis
Chemical Substances	Neonicotinoids ; Pesticide Residues ; Phenylurea Compounds ; Pyrazoles ; Pyridines ; Thiazines ; pyriproxyfen (3Q9VOR705O) ; thiacloprid (DSV3A944A4) ; tolfenpyrad (OHA74571QT) ; novaluron (Z8H1B3CW0B)
Language	English
Publishing date	2018-07-02
Publishing country	England
Document type	Journal Article
ZDB-ID	243123-3
ISSN	1873-7072 ; 0308-8146
ISSN (online)	1873-7072
ISSN	0308-8146
DOI	10.1016/j.foodchem.2018.07.005
Database	MEDical Literature Analysis and Retrieval System OnLINE

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Article: Control effect of hexaflumuron against the tomato late blight

Wen Guangyue, Shanghai Academy of Agricultural Sciences, Shanghai(China), Research Institute of Plant Protection / Zhang Sui, Shanghai Academy of Agricultural Sciences, Shanghai(China), Research Institute of Plant Protection / Zou Zhi, Shanghai Academy of Agricultural Sciences, Shanghai(China), Research Institute of Plant Protection

Plant Protection

Jun.2009 , Issue (3)

Abstract: 通过药效试验发现氟铃脲对番茄晚疫病有一定的防治效果。室内离体试验结果表明，氟铃脲对番茄晚疫病菌的EC50为65.69μg／mL盆栽试验结果表明，6.25-200μg／mL氟铃脲对番茄晚疫病均表现出一定的预防效果；田间小区试验200μg／mL氟铃脲对番茄晚疫病的防效达到了64.42％。[著者文摘] ...

Abstract	通过药效试验发现氟铃脲对番茄晚疫病有一定的防治效果。室内离体试验结果表明，氟铃脲对番茄晚疫病菌的EC50为65.69μg／mL盆栽试验结果表明，6.25-200μg／mL氟铃脲对番茄晚疫病均表现出一定的预防效果；田间小区试验200μg／mL氟铃脲对番茄晚疫病的防效达到了64.42％。[著者文摘]
Keywords	TOMATOES ; BLIGHT ; CONTROL METHODS ; TOMATE ; DEPERISSEMENT ; METHODE DE LUTTE ; TOMATE ; TIZON ; METODOS DE CONTROL ; http://www.fao.org/aos/agrovoc#c_7805 ; http://www.fao.org/aos/agrovoc#c_957 ; http://www.fao.org/aos/agrovoc#c_5728
Language	zho
Document type	Article
ISSN	0529-1542
Database	AGRIS - International Information System for the Agricultural Sciences and Technology

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